Table 2.
S. no | Name of the component | Chemical formula | Retention time (mins) | Relative abundance (%) |
---|---|---|---|---|
1 | Disiloxane, 1,3-bis(chloromethyl)-1,1,3,3-tetramethyl- | C6H16Cl2OSi2 | 7.197 | 0.9299 ± 0.5 |
2 | Carbamodithioic acid, phenyl-, methyl ester | C8H9NS2 | 7.291 | 0.003015 ± 0.1 |
3 | N-(Trimethylsilyl)acetamide | CH3CONHSi (CH3)3 | 7.3048 | 0.5491 ± 0.8 |
4 | 2-Butenoic acid, tert-butyldimethylsilyl ester | C17H36O3Si2 | 7.8719 | 0.15488 ± 0.1 |
5 | Formamide, N,N-diethyl- | HCON(C2H5)2 | 7.886 | 0.8218 ± 1.1 |
6 | Isoquinolin-6,7-diol, 1-methyl | C10H9NO2 | 8.2131 | 1.2960 ± 1.7 |
7 | 1-Hexene, 4,5-dimethyl- | C8H16 | 8.2312 | 1.30402 ± 0.1 |
8 | Sulfurous acid, di(cyclohexylmethyl) ester | C14H26O3S | 8.2767 | 0.01376 ± 0.1 |
9 | Azetidine, 1-acetyl-2-methyl- | C6H11NO | 8.2854 | 2.83459 ± 0.2 |
10 | Disilathiane, hexamethyl | C6H18SSi2 | 8.348 | 1.39148 ± 0.1 |
11 | 2,4,4-Trimethyl-1-hexene | C9H18 | 8.4016 | 0.4074 ± 0.6 |
12 | Acetamide, N-ethyl- | C4H9NO | 8.8449 | 0.3275 ± 0.5 |
13 | Tris(trimethylsilyl)borate | C9H27BO3Si3 | 9.1013 | 0.557147 ± 0.1 |
14 | 1,2-Bis(trimethylsiloxy)ethane | C8H22O2Si2 | 9.1285 | 0.8199 ± 1.1 |
15 | Silanol, trimethyl-, carbonate (2:1) | C7H18O3Si2 | 8.7307 | 0.3330 ± 0.5 |
16 | Acetamide, N-ethyl- | C4H9NO | 8.8449 | 0.3280 ± 0.5 |
17 | 1,2-Bis(trimethylsiloxy)ethane | C8H22O2Si2 | 9.1285 | 0.8200 ± 1.1 |
18 | Acetamide, N,N-diethyl- | C6H13NO | 9.5024 | 1.5998 ± 2.2 |
19 | 2,2-Diethylacetamide | C6H13NO | 10.0863 | 2.5606 ± 3.6 |
20 | Tris(trimethylsilyl)carbamate | C10H27NO2Si3 | 10.316 | 0.1908 ± 0.3 |
21 | N,N-Diethyl(trimethylsilyl)carbamate | C8H19NO2Si | 11.0868 | 0.2737 ± 0.4 |
22 | Propanoic acid, 2-[(trimethylsilyl)oxy]-, trimethylsilyl ester | C9H22O3Si2 | 11.2173 | 0.5037 ± 0.7 |
23 | Acetic acid, [(trimethylsilyl)oxy]-, trimethylsilyl ester | C8H20O3Si2 | 11.7152 | 1.2734 ± 1.8 |
24 | Isophorone | C9H14O | 13.1412 | 0.3485 ± 0.5 |
25 | Silanol, trimethyl-, phosphate (3:1) | C9H27O4PSi3 | 17.332 | 0.4860 ± 0.7 |
26 | Glycerol, tris(trimethylsilyl) ether | C12H32O3Si3 | 17.4314 | 0.8582 ± 1.2 |
27 | Butanedioic acid, bis(trimethylsilyl) ester | C10H22O4Si2 | 18.5644 | 0.3425 ± 0.5 |
28 | 2-(2-Butoxyethoxy)ethoxy-trimethylsilane | C11H26O3Si | 19.1932 | 0.2287 ± 0.3 |
29 | L-Proline, 5-oxo-1-(trimethylsilyl)-, trimethylsilyl ester | C11H23NO3Si2 | 23.7834 | 0.2626 ± 0.4 |
30 | Tricyclo[5.2.1.0(2,6)]decane, 3-methylene-4-phenyl | C17H20 | 27.9234 | 1.3391 ± 1.9 |
31 | 1,4-Benzenedicarboxylic acid, bis(trimethylsilyl) ester | C14H22O4Si2 | 29.9265 | 0.2885 ± 0.4 |
32 | 1-Nonadecene | C19H38 | 30.1214 | 0.1761363 ± 0.2 |
33 | Azelaic acid, bis(trimethylsilyl) ester | C15H32O4Si2 | 30.1519 | 0.1670219 ± 0.8 |
34 | D-(-)-Ribofuranose, tetrakis(trimethylsilyl) ether (isomer 2) | C17H42O5Si4 | 31.0492 | 0.6179 ± 0.9 |
35 | Salbutamol, N-trifluoroacetyl-O,O,o-tris(trimethylsilyl)deriv | C24H44F3NO4Si3 | 31.309 | 0.3250 ± 0.5 |
36 | α-D-Allopyranose, pentakis(trimethylsilyl) ether | C21H52O6Si5 | 32.3191 | 0.2874 ± 0.4 |
37 | Hexadecanoic acid, trimethylsilyl ester | C19H40O2Si | 35.1335 | 3.0713 ± 4.0 |
38 | 9,12-Octadecadienoic acid (Z,Z)-, trimethylsilyl ester | C21H40O2Si | 38.1093 | 3.3908 ± 4.7 |
39 | Oleic acid, trimethylsilyl ester | C21H42O2Si | 38.2218 | 1.7593 ± 2.4 |
40 | trans-9-Octadecenoic acid, trimethylsilyl ester | C21H42O2Si | 38.2268 | 7.27069 ± 0.8 |
41 | Octadecanoic acid, trimethylsilyl ester | C21H44O2Si | 38.7029 | 3.2747 ± 4.6 |
42 | Stearic acid, 2-(1-octadecenyloxy)ethyl ester, (Z)- | C38H74O3 | 42.4672 | 1.2604 ± 1.8 |
43 | Hexadecanoic acid, 2,3-bis[(trimethylsilyl)oxy]propyl ester | C25H54O4Si2 | 44.2692 | 0.4854 ± 0.7 |
44 | Chrysin, bis(trimethylsilyl) ether | C21H26O4Si2 | 44.6518 | 12.8317 ± 3.5 |
45 | Octadecanoic acid, 2,3-bis[(trimethylsilyl)oxy] propyl ester | C27H58O4Si2 | 47.0836 | 2.1723 ± 3.0 |
46 | .psi.,.psi.-Carotene, 1,1′,2,2′-tetrahydro-1,1′-dimethoxy- | C42H64O2 | 52.9052 | 0.0880 ± 0.1 |
Chrysin (highlighted in bold) was one of the myco-components detected in the ethyl acetate total culture extract of C. globosum. The components were identified by comparing the spectrum of the unknown components with the spectrum of reported components in the National Institute Standard and Technology (NIST) library. The relative abundance of each component was calculated by comparing its average peak area to the total area contributed by all the components.