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. Author manuscript; available in PMC: 2025 Mar 4.
Published in final edited form as: Chem Soc Rev. 2024 Mar 4;53(5):2603–2642. doi: 10.1039/d3cs00693j

Table 4.

Summary of glycan microarray studies for early detection and diagnosis of cancer

Cancer Type Array composition
Samples screened Key findings and glycan antigen hits Ref
Breast Cancer ~200 glycans and glycoproteins 18 patients, 15 healthy controls LacNAcs, Fuc-Core-2s, Sulfo-Core-2s, sTn
Antibodies to these glycans were significantly higher in all patients compared to healthy controls
220
Breast, Ovarian, Prostate 15 Glycosylated/ non-glycosylated MUC1 and MUC2 peptides 56 patients (ovarian, breast, prostate),
39 healthy controls
Tn-, sTn-, and Core 3-modified MUC1
IgG to these antigens was present in several cancer patient serum samples but absent in al healthy controls.
218
Breast Cancer 31 Glycosylated/ non-glycosylated MUC1 and MUC2 peptides 395 patients, 108 benign breast disease controls, 99 healthy controls Core 3-MUC1, sTn-MUC1
More then 30% of cancer patients demonstrated antibody binding to these antigens; whereas less than 15% of healthy controls yielded the same result.
224
Breast Cancer 11 Glycosylated/ non-glycosylated MUC1 and MUC2 peptides Total: 1036 patients, 1368 controls
Discovery: 273 patients, 273 controls
Validation: 431 patients, 431 controls
Third set: 332 patients, 664 controls
MUC1-Core 3, MUC1sTn, MUC1Tn
Antibodies to these antigens were observed to be elevated in cancer cases in the discovery set (however, the same trend was not observed in the validation set)
219
Breast Cancer 40 Sialic acid variants (Neu5Ac vs Neu5Gc) Discovery set: 87 patients, 25 healthy controls
Validation set: 74 patients, 25 controls
sTn with Neu5Gc sialylation
Antibody signals to this glycan demonstrated predictive power (AUC = 0.6 in ROC) for breast cancer detection.
132
Breast Cancer 8 Globo H and analogs 58 patients, 47 controls Globo H
IgG and IgM levels in cancer patient sera were roughly twice as high compared to healthy controls.
228
Ovarian Cancer 203 Synthetic glycans (mammalian, bacterial, and cancer-associated motifs) 33 patients, 24 healthy controls P1 and sialyl 6-sulfo LacNAc, 6-sialyl LacNAc, LN-6’LN, sTn, 6-sulfo-3’-sialyl TG
Antibody levels to this combination of antigens yielded better diagnostic sensitivity (79.2%) and specificity (84.8%) than the standard in the field. Interestingly, anti-P1 antibodies are lower in cancer cases.
230
Ovarian Cancer 203 Synthetic glycans (mammalian, bacterial, and cancer-associated motifs) 74 patients, 81 controls P blood group glycans (Pk, P, and P1)
These antigens were observed to be expressed in cancer tissue samples. Interestingly, anti-P1 antibodies are lower in cancer cases.
231
Ovarian Cancer 3 Glycans (Globo H + 1 positive control + 1 negative control) 19 patients, 29 controls Globo H
IgG to this antigen, when used in tandem with CA-125 levels, improved diagnostic accuracy when compared to the standard (CA-125 alone).
232
Ovarian Cancer 22 Sialylated and sulfated glycans 22 patients, 31 controls sTn, 6-Osulfo-TF, 6-Osulfo-LacNAc, sLeA, GM2
Antibodies against these glycans, alongside CA-125 levels, detected almost all cancer cases (AUC = 0.9853 in ROC).
233
Colorectal Cancer Array 1 (“glycochip”): 7 glycan antigens + 3 anti-human antibodies

Array 2 (“oncochip”): 6 anti-glycan antibodies
33 patients, 67 healthy conors, 27 IBD patients Tn, TF, sLeA, Manβ1–4GlcNAc
Collective antibody signature to these four antigens—as determined by “glycochip” array analysis—determined “good predictive mutual capacity,” with AUC = 0.747 on ROC curve.
235
Colorectal Cancer 51 glycan antigens (various types) 44 patients, 53 healthy controls 3’-O-sulfo-LeA and 3’sialyl-TF
Antibodies to these antigens identified 74.3% of cancer cases in the cohort.
236
Colorectal Cancer 49 Mucin glycopeptides and glycoproteins 58 patients, 39 IBD patients, 50+53 healthy controls Tn-, sTn-, and Core 3-modified MUC1
IgG to these antigens was observed in ~75% of screened cancer serum samples.
237
Colorectal Cancer 62 Sialylated glycans (Neu5Gc vs Neu5Ac) 71 patients, 71 healthy controls Neu5Gc-containing glycans
High cumulative IgG signal to Neu5Gc-containing glycans was associated with incidence of colorectal cancer.
137
Prostate Cancer 64 N-glycans (glycoproteins, synthetic glycans, glycolipids, non-human glycans) 17 patients, 12 controls Man-9, OR-ASOR
Levels of antibodies to these glycans were significantly higher in cancer patients relative to controls
241
Liver Cancer 2 AFP glycoforms (AFP-L1 and AFP-L3) 32 patients, 8 hepatitis B patients AFP-L3
Antibody signals to this antigen were significantly higher in patients compared to controls.
245
Liver Cancer 58 Synthetic glycans 293 patients, 133 hepatitis B patients, 134 hepatitis C patients, 33 healthy Sialyl LacNAc 6SO₃, DSGG, Fuc-GM1, Gb3, Gb2, B19, and Man7
IgG levels to these antigens were significantly elevated relative to controls
246
Lymphoma 37 Human and plant glycans 8 patients, unspecified nuymber of healthy controls L-Araf, Fuc(α), Fuc(α1–2)Gal-β, Tn, and GalNAc(β)
Antibody signal to these glycans was elevated compared to in controls
249
Gastric Cancer 300 glycan antigens (various types) 146 patients, 55 healthy controls KDNβ1–6’LN-C3, β1–3’SLN, LN-C8, Aα1–4A, TF, 3’Sialyl-LeC and Tn3Su
IgM to these antigens elicited a significant signal.

GN6Su, TF, para-Fs and βGU
IgG to these antigens elicited a significant signal.
252
Pancreatic Cancer 609 glycan antigens (various types) 14 patients, 6 controls Terminal GlcNAcα1–4Galβ1–4GlcNAc
This motif was present in half of the glycans eliciting an antibody signal in this array.
258
OSCC 22 glycan antigens (various types) 65 patients, 21 healthy controls. SSEA-3, GD2
IgM signal to these antigens was elevated in cancer patients relative to controls.

GD2, GloboH, LeY, sLeX
IgG signal to these antigens was reduced in cancer patients relative to controls.
261