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Details on the reaction conditions that were used to optimise the polymerisation of diethyl pyridine-2,4-dicarboxylate (PD24) and 1,8-octanediol (ODO) using the new green solvents (anisole, eucalyptol, cyclohexanone, or phenetole) and CaLB as the biocatalyst.
| Condition | Total time (h) | Time at 1000 mbar (h) | Time at 360 mbar (h) |
|---|---|---|---|
| 1 | 96 | 96 | 0 |
| 2 | 48 | 6 | 42 |
| 3 | 72 | 6 | 66 |
