Table 1.
Data processing and refinement statistics for ADAR2-R2D E488Q:GLI1 8-AN 32mer PDB: 6VFF
| Synchrotron (beamline) | SSRL (12–2) |
|---|---|
| Wavelength (Å) | 0.97946 |
| Space group | C2 |
| Unit cell parameters (Å) | a = 170.0, b = 63.21, c = 142.20 |
| Resolution range (Å) | 37.48–2.80 (2.87–2.80) |
| No. observed reflections | 178 826 (12 253) |
| No. unique reflections | 32 384 (2260) |
| Completeness (%) | 97.3 (92.1) |
| I/σ (I) | 14.14 (1.56) |
| R merge a (%) | 9.4 (118.1) |
| CC1/2 | 99.8 (61.1) |
| Refinement statistics | |
| Rfactorb (%) | 0.1965 |
| Rfreeb (%) | 0.2483 |
| RMS bond length (Å) | 0.008 |
| RMS bond angle (°) | 1.247 |
| Ramachandran plot statistics c | |
| Favored (%) | 93.09 |
| Allowed (%) | 5.06 |
| Outliers (%) | 1.85 |
| No. of atoms | |
| Protein | 6403 |
| RNA | 1357 |
| Inositol hexakisphosphate (IHP) | 72 |
| Zn | 2 |
| Waters | 36 |
| B factors | |
| Protein | 78.36 |
| RNA | 97.23 |
| IHP | 63.44 |
| Zn | 56.79 |
| Water | 62.10 |
a R merge = [∑h∑i|Ih – Ihi|/∑h∑iIhi] where Ih is the mean of Ihi observations of reflection h. Numbers in parenthesis represent highest resolution shell.
b R-factor and cRfree = ∑||Fobs| – |Fcalc|| / ∑|Fobs| x 100 for 95% of recorded data (R-factor) or 5% data (Rfree).
cRamachandran plot statistics from MolProbity (73).