Table 1. Data collection and processing.
| LCP crystallization | LSP co-crystallization with carotenoid | In surfo structure | |
|---|---|---|---|
| Diffraction source | ESRF, beamline ID23-1 | PETRA III, DESY beamline P11 | BESSY, beamline BL14.1 |
| Wavelength (Å) | 0.8610 | 1.033 | 0.9184 |
| Photon flux at sample [photons s−1 (100 mA)−1] | 4 × 1012 | 8 × 1012 | 1.4 × 1011 |
| Temperature (K) | 100 | 100 | 100 |
| Detector | Dectris PILATUS3 S 6M pixel | Dectris PILATUS3 S 6M pixel | Dectris PILATUS3 S 6M pixel |
| Crystal–detector distance (mm) | 426 | 413 | 236 |
| Rotation range per image (°) | 0.05 | 0.1 | 0.1 |
| Total rotation range (°) | 150 | 150 | 180 |
| Exposure time per image (s) | 0.037 | 0.05 | 2 |
| Space group | P42212 | P42212 | P3121 |
| a, b, c (Å) | 99.9, 99.9, 234.1 | 99.9, 99.9, 238.5 | 139.9, 139.9, 185.4 |
| α, β, γ (°) | 90, 90, 90 | 90, 90, 90 | 90, 90, 120 |
| Mosaicity (°) | 0.05 | 0.053 | 0.14 |
| Resolution range (Å) | 50.0–2.07 (2.13–2.07) | 50–2.1 (2.15–2.1) | 50–2.1 (2.2–2.1) |
| Total No. of reflections | 802655 (62473) | 778321 (48871) | 579056 (56011) |
| No. of unique reflections | 72564 (5862) | 71322 (5199) | 121690 (15297) |
| Completeness (%) | 99.9 (100.0) | 99.9 (100.0) | 99.5 (96.9) |
| Redundancy | 11.06 (10.66) | 10.91 (9.40) | 4.75 (3.66) |
| 〈I/σ(I)〉 | 15.94 (1.14) | 9.61 (1.31) | 12.52 (1.94) |
| R r.i.m. | 0.075 (184.6) | 0.199 (133.2) | 0.079 (68.8) |
| Overall B factor from Wilson plot (Å2) | 52.20 | 35.59 | 36.1 |