Table 1. Reaction Conditions of F-Ph-Terminated PC3SI.

polycondensation						cap reaction
run	feed j	C3F (g)	C3A (g)	DIPEA (mL)	MeCN (mL)	PC3SI (g)	FPhSO2Cl (g)	DIPEA (mL)	MeCN (mL)
1	5	13.8	20.3	38	40	16.9	5.33	20	20
2	15	18.1	20.3	50	20	39.3	5.00	30	30