Table 3. Comparison of Experimental and Predicted Values Using Box–Behnken Design for the Four Independent Variables on the Content of Polyphenol from Aqueous Acetone Extraction.
extraction temperature (°C) | extraction time (min) | solvent composition (%) | liquid–solid ratio | experimental value (%) | predicted value (%) | |
---|---|---|---|---|---|---|
test N | T | t | C | V | content | eq 1 |
1 | 50 | 90 | 20 | 20 | 9 | 9.61 |
2 | 50 | 90 | 100 | 20 | 10 | 10.23 |
3 | 50 | 90 | 60 | 20 | 13 | 10.11 |
4 | 45 | 120 | 40 | 25 | 13 | 12.57 |
5 | 50 | 150 | 60 | 20 | 13 | 13.57 |
6 | 50 | 90 | 60 | 20 | 10 | 10.23 |
7 | 55 | 120 | 40 | 25 | 9 | 8.61 |
8 | 55 | 120 | 80 | 15 | 12 | 14.19 |
9 | 50 | 90 | 60 | 10 | 7 | 10.11 |
10 | 55 | 60 | 40 | 25 | 8 | 9.61 |
11 | 45 | 120 | 40 | 15 | 8 | 10.23 |
12 | 45 | 120 | 80 | 15 | 7 | 8.52 |
13 | 60 | 90 | 60 | 20 | 9 | 7.90 |
14 | 45 | 60 | 80 | 25 | 14 | 14.19 |
15 | 50 | 30 | 60 | 20 | 10 | 8.52 |
16 | 55 | 60 | 80 | 25 | 13 | 11.11 |
17 | 55 | 60 | 40 | 15 | 12 | 10.23 |
18 | 45 | 120 | 80 | 25 | 11 | 11.73 |
19 | 55 | 60 | 80 | 15 | 9 | 8.61 |
20 | 50 | 90 | 60 | 30 | 7 | 8.73 |
21 | 40 | 90 | 60 | 20 | 13 | 12.69 |
22 | 50 | 90 | 60 | 20 | 15 | 12.69 |
23 | 45 | 60 | 40 | 15 | 12 | 10.23 |
24 | 45 | 60 | 40 | 25 | 7 | 7.02 |
25 | 45 | 60 | 80 | 15 | 11 | 10.23 |
26 | 55 | 120 | 40 | 15 | 7 | 7.02 |
27 | 55 | 120 | 80 | 25 | 11 | 11.11 |
28 | 50 | 90 | 60 | 20 | 6 | 6.90 |