Table 4. Comparison of Experimental and Predicted Values Using the Box-Behnken Design for the Four Independent Variables on the Content of Polyphenol from Aqueous Ethanol Extraction.
extraction temperature (°C) | extraction time (min) | solvent composition (%) | liquid–solid ratio | experimental value (%) | predicted value (%) | |
---|---|---|---|---|---|---|
test N | T | t | C | V | content | eq 2 |
1 | 60 | 90 | 20 | 20 | 12 | 15.15 |
2 | 60 | 90 | 100 | 20 | 12 | 15.47 |
3 | 60 | 90 | 60 | 20 | 10 | 15.31 |
4 | 50 | 120 | 40 | 25 | 19 | 12.58 |
5 | 60 | 150 | 60 | 20 | 14 | 17.77 |
6 | 60 | 90 | 60 | 20 | 13 | 15.31 |
7 | 70 | 120 | 40 | 25 | 14 | 20.16 |
8 | 70 | 120 | 80 | 15 | 16 | 16.31 |
9 | 60 | 90 | 60 | 10 | 13 | 11.90 |
10 | 70 | 60 | 40 | 25 | 19 | 19.50 |
11 | 50 | 120 | 40 | 15 | 10 | 10.97 |
12 | 50 | 120 | 80 | 15 | 20 | 13.53 |
13 | 80 | 90 | 60 | 20 | 13 | 16.89 |
14 | 50 | 60 | 80 | 25 | 19 | 14.48 |
15 | 60 | 30 | 60 | 20 | 18 | 12.85 |
16 | 70 | 60 | 80 | 25 | 17 | 17.26 |
17 | 70 | 60 | 40 | 15 | 14 | 14.29 |
18 | 50 | 120 | 80 | 25 | 15 | 15.14 |
19 | 70 | 60 | 80 | 15 | 10 | 12.05 |
20 | 60 | 90 | 60 | 30 | 16 | 18.72 |
21 | 40 | 90 | 60 | 20 | 16 | 6.53 |
22 | 60 | 90 | 60 | 20 | 15 | 15.31 |
23 | 50 | 60 | 40 | 15 | 13 | 6.71 |
24 | 50 | 60 | 40 | 25 | 19 | 11.92 |
25 | 50 | 60 | 80 | 15 | 12 | 9.27 |
26 | 70 | 120 | 40 | 15 | 15 | 18.55 |
27 | 70 | 120 | 80 | 25 | 17 | 17.92 |
28 | 60 | 90 | 60 | 20 | 12 | 15.31 |