Table 5. Comparison of Experimental and Predicted Values Using the Box-Behnken Design for the Four Independent Variables on the Content of Polyphenol from Aqueous NaOH Extraction.
extraction temperature (°C) | extraction time (min) | solvent composition (%) | liquid–solid ratio | experimental value (%) | predicted value (%) | |
---|---|---|---|---|---|---|
test N | T | t | C | V | content | eq 3 |
1 | 80 | 45 | 0.05 | 20 | 20 | 19.73 |
2 | 80 | 45 | 1.50 | 20 | 28 | 27.01 |
3 | 80 | 45 | 0.50 | 20 | 28 | 25.10 |
4 | 60 | 60 | 0.10 | 25 | 27 | 27.01 |
5 | 80 | 90 | 0.50 | 20 | 28 | 22.19 |
6 | 80 | 45 | 0.50 | 20 | 23 | 27.32 |
7 | 90 | 60 | 0.10 | 25 | 26 | 24.85 |
8 | 90 | 60 | 1.00 | 15 | 27 | 23.56 |
9 | 80 | 45 | 0.50 | 10 | 26 | 24.75 |
10 | 90 | 30 | 0.10 | 25 | 18 | 27.21 |
11 | 60 | 60 | 0.10 | 15 | 27 | 24.85 |
12 | 60 | 60 | 1.00 | 15 | 30 | 27.32 |
13 | 100 | 45 | 0.50 | 20 | 27 | 24.75 |
14 | 60 | 30 | 1.00 | 25 | 21 | 23.56 |
15 | 80 | 15 | 0.50 | 20 | 23 | 23.56 |
16 | 90 | 30 | 1.00 | 25 | 24 | 24.55 |
17 | 90 | 30 | 0.10 | 15 | 25 | 23.56 |
18 | 60 | 60 | 1.00 | 25 | 19 | 23.56 |
19 | 90 | 30 | 1.00 | 15 | 28 | 27.21 |
20 | 80 | 45 | 0.50 | 30 | 25 | 23.56 |
21 | 40 | 45 | 0.50 | 20 | 28 | 25.34 |
22 | 80 | 45 | 0.50 | 20 | 25 | 24.55 |
23 | 60 | 30 | 0.10 | 15 | 33 | 32.81 |
24 | 60 | 30 | 0.10 | 25 | 15 | 19.73 |
25 | 60 | 30 | 1.00 | 15 | 22 | 24.12 |
26 | 90 | 60 | 0.10 | 15 | 25 | 22.19 |
27 | 90 | 60 | 1.00 | 25 | 18 | 20.01 |
28 | 80 | 45 | 0.50 | 20 | 20 | 22.03 |