Bruker APEXII CCD diffractometer | 2463 independent reflections |
Radiation source: fine-focus sealed tube | 2126 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.026 |
Detector resolution: 8.3333 pixels mm-1 | θmax = 30.5°, θmin = 2.3° |
φ and ω scans | h = −12→12 |
Absorption correction: multi-scan (SADABS; Bruker, 2017) | k = −14→14 |
Tmin = 0.89, Tmax = 0.98 | l = −13→13 |
19282 measured reflections |