| Refinement on F2 | Primary atom site location: dual |
| Least-squares matrix: full | Secondary atom site location: difference Fourier map |
| R[F2 > 2σ(F2)] = 0.034 | Hydrogen site location: mixed |
| wR(F2) = 0.103 | H atoms treated by a mixture of independent and constrained refinement |
| S = 1.07 | w = 1/[σ2(Fo2) + (0.0559P)2 + 0.2301P] where P = (Fo2 + 2Fc2)/3 |
| 2463 reflections | (Δ/σ)max < 0.001 |
| 139 parameters | Δρmax = 0.50 e Å−3 |
| 0 restraints | Δρmin = −0.26 e Å−3 |