Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [CuCl2(C6H7N)2(CH4O)] |
| M r | 352.73 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 120 |
| a, b, c (Å) | 14.4554 (4), 8.5865 (2), 24.8055 (8) |
| β (°) | 99.209 (3) |
| V (Å3) | 3039.22 (16) |
| Z | 8 |
| Radiation type | Mo Kα |
| μ (mm−1) | 1.78 |
| Crystal size (mm) | 0.21 × 0.16 × 0.11 |
| Data collection | |
| Diffractometer | Agilent XCalibur diffractometer |
| Absorption correction | Multi-scan (CrysAlis PRO; Rigaku OD, 2018 ▸) |
| T min, T max | 0.549, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 15974, 5137, 4251 |
| R int | 0.040 |
| (sin θ/λ)max (Å−1) | 0.758 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.038, 0.081, 1.13 |
| No. of reflections | 5137 |
| No. of parameters | 178 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.54, −0.51 |