| Bruker D8 Quest with a Photon 100 CMOS detector diffractometer | 7596 independent reflections |
| Radiation source: sealed tube | 5005 reflections with I > 2σ(I) |
| Curved-graphite monochromator | Rint = 0.076 |
| Detector resolution: 8 pixels mm-1 | θmax = 28.4°, θmin = 2.9° |
| φ and ω scans | h = −19→19 |
| Absorption correction: multi-scan (SADABS; Bruker, 2016) | k = −46→46 |
| Tmin = 0.341, Tmax = 0.431 | l = −7→7 |
| 31843 measured reflections |