Table 3. Experimental details.
| Crystal data | |
| Chemical formula | [Cu2(NCS)2(C9H16N2S)2] |
| M r | 611.83 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 173 |
| a, b, c (Å) | 13.9881 (5), 9.8220 (4), 9.7446 (4) |
| β (°) | 91.391 (6) |
| V (Å3) | 1338.43 (9) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 1.92 |
| Crystal size (mm) | 0.15 × 0.15 × 0.1 |
| Data collection | |
| Diffractometer | Rigaku R-AXIS RAPID |
| Absorption correction | Multi-scan (ABSCOR; Higashi, 1995 ▸) |
| T min, T max | 0.747, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 12737, 3071, 2516 |
| R int | 0.041 |
| (sin θ/λ)max (Å−1) | 0.649 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.045, 0.098, 1.08 |
| No. of reflections | 3071 |
| No. of parameters | 168 |
| No. of restraints | 1 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.61, −0.40 |