| Refinement on F2 | Hydrogen site location: inferred from neighbouring sites |
| Least-squares matrix: full | H-atom parameters constrained |
| R[F2 > 2σ(F2)] = 0.048 | w = 1/[σ2(Fo2) + (0.0546P)2 + 0.3025P] where P = (Fo2 + 2Fc2)/3 |
| wR(F2) = 0.134 | (Δ/σ)max < 0.001 |
| S = 1.07 | Δρmax = 1.01 e Å−3 |
| 3572 reflections | Δρmin = −0.34 e Å−3 |
| 161 parameters | Extinction correction: SHELXL-2014/7 (Sheldrick 2014, Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
| 0 restraints | Extinction coefficient: 0.091 (17) |
| Primary atom site location: structure-invariant direct methods |