| Crystal data |
| Chemical formula |
(C10H10N3)2[Ni(CN)4] |
|
M
r
|
507.21 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
273 |
|
a, b, c (Å) |
7.1046 (4), 9.1467 (4), 9.3833 (4) |
| α, β, γ (°) |
100.182 (2), 98.729 (2), 97.444 (2) |
|
V (Å3) |
585.49 (5) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.86 |
| Crystal size (mm) |
0.35 × 0.23 × 0.19 |
| |
| Data collection |
| Diffractometer |
Oxford Diffraction Xcalibur with Sapphire CCD detector |
| Absorption correction |
Multi-scan (CrysAlis RED; Oxford Diffraction, 2009 ▸) |
|
T
min, T
max
|
0.914, 0.962 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
16272, 3572, 2659 |
|
R
int
|
0.052 |
| (sin θ/λ)max (Å−1) |
0.715 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.048, 0.134, 1.07 |
| No. of reflections |
3572 |
| No. of parameters |
161 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.01, −0.34 |
