Oxford Diffraction Xcalibur with Sapphire CCD diffractometer | 3838 independent reflections |
Radiation source: Enhance (Mo) X-ray Source | 2600 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.013 |
ω scans | θmax = 27.7°, θmin = 2.7° |
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) | h = −5→10 |
Tmin = 0.883, Tmax = 0.968 | k = −11→13 |
6091 measured reflections | l = −15→15 |