| Oxford Diffraction Xcalibur with Sapphire CCD diffractometer | 3668 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 2606 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.014 |
| ω scans | θmax = 27.6°, θmin = 2.7° |
| Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) | h = −18→15 |
| Tmin = 0.830, Tmax = 0.986 | k = −5→9 |
| 6720 measured reflections | l = −17→20 |