| Refinement on F2 | Hydrogen site location: mixed |
| Least-squares matrix: full | H atoms treated by a mixture of independent and constrained refinement |
| R[F2 > 2σ(F2)] = 0.040 | w = 1/[σ2(Fo2) + (0.0587P)2 + 0.1566P] where P = (Fo2 + 2Fc2)/3 |
| wR(F2) = 0.119 | (Δ/σ)max < 0.001 |
| S = 1.07 | Δρmax = 0.24 e Å−3 |
| 4279 reflections | Δρmin = −0.27 e Å−3 |
| 317 parameters | Extinction correction: SHELXL, Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
| 85 restraints | Extinction coefficient: 0.021 (3) |
| Primary atom site location: difference Fourier map |