Oxford Diffraction Xcalibur with Sapphire CCD diffractometer | 3763 independent reflections |
Radiation source: Enhance (Mo) X-ray Source | 2318 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.019 |
ω scans | θmax = 27.5°, θmin = 2.6° |
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) | h = −9→8 |
Tmin = 0.884, Tmax = 0.963 | k = −10→6 |
6241 measured reflections | l = −19→19 |