Oxford Diffraction Xcalibur with Sapphire CCD diffractometer | 3307 independent reflections |
Radiation source: Enhance (Mo) X-ray Source | 2608 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.009 |
ω scans | θmax = 27.8°, θmin = 2.6° |
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) | h = −10→5 |
Tmin = 0.867, Tmax = 0.967 | k = −11→11 |
5533 measured reflections | l = −13→14 |