| Rigaku R-AXIS RAPIDII diffractometer | 4365 reflections with I > 2σ(I) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.017 |
| ω scans | θmax = 30.0°, θmin = 3.0° |
| Absorption correction: numerical (NUMABS; Higashi, 1999) | h = −10→9 |
| Tmin = 0.938, Tmax = 0.955 | k = −10→10 |
| 30061 measured reflections | l = −39→40 |
| 4532 independent reflections |