| Crystal data |
| Chemical formula |
[Au(C26H24P2S2)][AuBr2] |
|
M
r
|
1016.26 |
| Crystal system, space group |
Monoclinic, C2/c
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
21.4112 (8), 11.9708 (2), 13.7726 (4) |
| β (°) |
128.316 (7) |
|
V (Å3) |
2769.7 (3) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
25.63 |
| Crystal size (mm) |
0.12 × 0.005 × 0.005 |
| |
| Data collection |
| Diffractometer |
Oxford Diffraction Xcalibur, Atlas, Nova |
| Absorption correction |
Multi-scan (CrysAlis PRO; Oxford Diffraction, 2010 ▸) |
|
T
min, T
max
|
0.387, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
27632, 2873, 2630 |
|
R
int
|
0.037 |
| (sin θ/λ)max (Å−1) |
0.629 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.021, 0.053, 1.06 |
| No. of reflections |
2873 |
| No. of parameters |
155 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.42, −0.99 |
