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. 2020 Oct 6;76(Pt 11):1716–1719. doi: 10.1107/S2056989020013201

Table 2. Experimental details.

Crystal data
Chemical formula TlMgCl3
M r 335.03
Crystal system, space group Hexagonal, P63/m m c
Temperature (K) 290
a, c (Å) 7.0228 (4), 17.4934 (15)
V3) 747.18 (11)
Z 6
Radiation type Mo Kα
μ (mm−1) 33.97
Crystal size (mm) 0.10 × 0.10 × 0.10
 
Data collection
Diffractometer Bruker Kappa APEXII CCD
Absorption correction Multi-scan (SADABS; Bruker, 2004)
T min, T max 0.578, 0.746
No. of measured, independent and observed [I > 2σ(I)] reflections 4109, 489, 387
R int 0.047
(sin θ/λ)max−1) 0.718
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.047, 0.113, 1.42
No. of reflections 489
No. of parameters 21
Δρmax, Δρmin (e Å−3) 1.88, −2.11

Computer programs: APEX2 and SAINT (Bruker, 2004), SHELXT2014/4 (Sheldrick, 2015a ), SHELXL2018/3 (Sheldrick, 2015b ) and VESTA (Momma & Izumi, 2011).