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. 2020 Nov 5;11:5599. doi: 10.1038/s41467-020-19407-3

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© The Author(s) 2020

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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Fig. 4 — a GPC curves of poly(methyl acrylate) (PMA) and polystyrene (PS) obtained by enzyme-degassed Pickering emulsion SET-LRP. Reaction conditions: [Monomer]₀/[MBPA or EBiB]₀/[Me₆-TREN]₀/[Cu(0)]₀ = 200/1/0.2/0.3. [Lignin nanoparticles] = 2.25 wt% relative to MA or S. b Dependence of experimental M_n (GPC) and M_w/M_n on the [BMA]₀/[MBPA]₀ ratio. The mean values ± SD (n = 2) of BMA conversion for the different DPs are given in Supplementary Fig. 13, whereas all data points are shown in b. c GPC analysis of block copolymerization via purification-reinitiation strategy of poly(butyl methacrylate) (PBMA) with styrene (S) to synthetize a PBMA-PS block copolymer. Reaction conditions for the PBMA macroinitiator: [BMA]₀/[MBPA]₀/[Me₆-TREN]₀/[Cu(0)]₀ = 50/1/0.2/0.3. [GOx-chi-LNPs] = 2.25 wt% relative to BMA.