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. 2020 Oct 20;23(11):101702. doi: 10.1016/j.isci.2020.101702

Table 1.

Employing Different Phenols

Entry R1/R2/R3(2) 3 Yield (%)a
1 H/H/H(2a) 3a 59
2 H/Cl/H(2b) 3b 33
3 H/H/Cl(2c) 3c 36
4 Cl/H/Cl(2d) 3d 30.
5 H/H/Br(2e) 3e 21
6 Br/H/Br(2f) 3f 39
7 H/H/I(2g) 3g <10

Reaction conditions: 1 (55 mmol), 2 (50. mmol), Et3N (55 mmol) in CH2Cl2 (40 mL) at room temperature and under dry nitrogen atmosphere for 24 h with spectroscopic and physical characterization provided in Data S1 and S2.

See also Figure S9.

a

Yields refer to average isolated yields.