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. 2020 Oct 26;8:596889. doi: 10.3389/fchem.2020.596889

Table 1.

13C NMR (100 MHz) data of compounds 1~14.

Position 1a 2a 3a 4a 5a 6a 7a 8a 9a 10a 11a 12a 13c 14a 14b
1 65.2, CH 76.4, CH 78.7, CH 129.06, CHd 74.3, CH 32.6, CH2 128.5, CH 65.5, CH 32.6, CH2 58.1, CH 146.4, C 127.8, CH 124.7, CH 114.7, CH 113.5, CH
2 43.8, CH2 72.3, CH 72.1, CH 136.1, CH 35.1, CH2 41.8, CH2 135.9, CH 44.5, CH2 40.6, CH2 61.3, CH 176.3, C 181.4, C 192.6, C 167.0, C 163.5, C
3 72.3, CH 34.3, CH2 77.6, CH 74.3, CH 26.2, CH2 211.4, C 74.2, CH 72.0, CH 212.1, C 73.7, CH 145.5, C 146.7, C 72.8, CH - -
4 47.1, CH 41.1, CH 45.0, CH 75.0, C 48.7, CH 57.4, CH 76.1, C 46.7, CH 54.3, CH 82.0, C 135.9, C 136.0, C 42.3, CH 106.8, C 104.9, C
5 43.5, C 41.7, C 40.8, C 44.6, C 41.6, C 43.6, C 43.5, C 41.4, C 43.2, C 44.5, C 41.7, C 46.9, C 38.8, C 43.7, C 41.6, C
6 43.7, CH2 43.4, CH2 44.7, CH2 35.9, CH2 48.8, CH2 44.2, CH2 39.5, CH2 42.8, CH2 40.7, CH2 39.1, CH2 33.0, CH2 32.9, CH2 33.8, CH2 29.9, CH2 28.2, CH2
7 128.9, C 129.3, C 128.9, C 129.7, C 78.9, C 78.2, C 78.6, C 77.3, C 76.7, C 77.3, C 147.5, C 142.4, C 139.0, C 139.9, C 138.1, C
8 194.4, C 194.4, C 194.0, C 194.1, C 205.2, C 203.3, C 203.6, C 202.8, C 201.5, C 200.0, C 151.2, C 148.0, C 142.2, C 144.7, C 142.9, C
9 122.6, CH 130.7, CH 130.7, CH 129.10, CHd 123.5, CH 123.2, CH 124.8, CH 118.5, CH 124.3, CH 126.5, CH 103.6, C 174.8, C 107.4, C 106.0, CH 103.8, CH
10 174.0, C 168.1, C 167.2, C 162.1, C 169.3, C 166.8, C 162.2, C 175.6, C 167.9, C 168.7, C 131.8, C 161.3, C 163.9, C 159.8, C 157.1, C
11 145.2, C 146.0, C 147.2, C 146.8, C 33.5, CH 33.6, CH 33.6, CH 35.1, CH 34.8, CH 77.3, C 125.1, C 124.2, C 129.2, C 129.7, C 127.7, C
12 22.8, CH3 22.9, CH3 23.0, CH3 23.2, CH3 15.9, CH3 16.4, CH3 16.5, CH3 16.2, CH3 16.1, CH3 27.3, CH3 172.3, C 149.5, CH 173.1, C 174.9, C 172.2, C
13 22.3, CH3 22.5, CH3 22.7, CH3 22.8, CH3 17.0, CH3 16.8, CH3 16.9, CH3 17.8, CH3 18.1, CH3 26.6, CH3 8.5, CH3 7.5, CH3 8.5, CH3 8.2, CH3 8.1, CH3
14 20.2, CH3 18.6, CH3 21.5, CH3 22.1, CH3 19.8, CH3 20.6, CH3 23.8, CH3 25.8, CH3 23.1, CH3 22.4, CH3 29.1, CH3 25.9, CH3 23.3, CH3 24.6, CH3 23.9, CH3
15 12.3, CH3 15.4, CH3 12.3, CH3 19.8, CH3 15.1, CH3 7.5, CH3 19.8, CH3 12.5, CH3 8.0, CH3 21.1, CH3 11.3, CH3 11.2, CH3 10.3, CH3 22.3, CH3 21.9, CH3
-OAc 169.9, C,
20.8, CH3

Recorded in

a

CD3OD;

b

DMSO-d6;

c

CDCl3.

d

assignments within a column might be interchanged.