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. 2020 Nov 9;35(1):1937–1943. doi: 10.1080/14756366.2020.1837123

Scheme 1.

Scheme 1.

Synthetic route for the preparation of compounds 4a-4c and precursors. Reagents and conditions: (i) microwave, DMF, stirred at 100 W for 1 h; (ii) acetonitrile, pyridine, stirred for 1–2 h, room temperature; (iii) oxalyl chloride, stirred for 30 min, room temperature.