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. 2020 Oct 30;11:599911. doi: 10.3389/fmicb.2020.599911

TABLE 1.

1H and 13C NMR spectral data for lenzimycins A and B (1-2) in CDCl3.

Position 1a
2b
δC Type δH, mult (J in Hz) δC Type δH, mult (J in Hz)
1 173.8 C 173.3 C
2 34.1 CH2 2.30 t (7.7) 34.3 CH2 2.30 t (7.0)
3 24.9 CH2 1.60 m 24.9 CH2 1.60 m
4–10 30.0-27.1 CH2 1.31-1.23 m 30.0-27.1 CH2 1.31-1.23 m
11 36.6 CH2 1.27, 1.07 m 36.6 CH2 1.27, 1.07 m
12 34.4 CH 1.28 m 34.4 CH 1.28 m
12-Me 19.2 CH3 0.83 t (6.5) 19.2 CH3 0.84 t (6.5)
13 29.5 CH2 1.25, 1.12 m 29.5 CH2 1.25, 1.12 m
14 11.4 CH3 0.84 t (7.2) 11.4 CH3 0.85 t (7.2)
1′ 64.5 CH2 4.11 m 59.8 CH2 3.73 d (5.3)
2′ 69.1 CH 3.98 m 72.5 CH 4.97 m
3′ 68.1 CH2 4.00, 3.90 m 63.4 CH2 4.08 m
1″″ 61.6 CH2 4.19 m 61.2 CH2 4.20 m
2″ 49.7 CH2 3.15 m 49.9 CH2 3.14 m
2″-NH 9.64 br s 9.73 br s
2″-N-Me 33.6 CH3 2.70 s 33.7 CH3 2.71 s

a1H and 13C NMR were recorded at 800 MHz and 200 MHz, respectively.b1H and 13C NMR were recorded at 850 MHz and 212.5 MHz, respectively.