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Crystallinity index and crystallite size of CNCs produced under different hydrolysis conditions.
| Temperature (°C) | Reaction time (min) | Sulfuric acid concentration (%) | Crystallinity (%) | Crystallite size (nm) |
|---|---|---|---|---|
| 45 | 30 | 58 | 90.77 | 5.33 |
| 55 | 30 | 58 | 87.99 | 4.95 |
| 65 | 30 | 58 | 80.32 | 4.73 |
| 45 | 45 | 58 | 87.55 | 5.22 |
| 45 | 60 | 58 | 83.52 | 4.62 |
