Table 1. Elemental Surface Concentrations and Relative Abundance of Carbon Bonds for the Plasma-Modified TEMPO-CNF Films Analyzed Using XPSa.
elemental concentrations [atom %] |
relative abundance of carbon bonds [atom %] |
|||||||||
---|---|---|---|---|---|---|---|---|---|---|
sample | C 1s | O 1s | N 1s | Si 2p | O/Si | C/Si | C–C/C–Si | C–O | O–C–O | O–C=O |
ref TEMPO-CNF | 54.5 | 41.1 | 0.5 | 2.6 | 11.9 | 67.8 | 17.1 | 3.2 | ||
HMDSO | 44.9 | 36.2 | 0.4 | 18.4 | 2.0 | 2.4 | 45.4 | 43.3 | 10.0 | 1.2 |
APTES | 53.2 | 27.3 | 5.5 | 14.0 | 2.0 | 3.8 | 52.4 | 37.9 | 9.2 | 0.5 |
APTES + HMDSO | 35.8 | 35.7 | 3.5 | 24.9 | 1.4 | 1.4 | 65.9 | 21.0 | 6.7 | 6.4 |
Values are given in atomic percentage as an average of at least two measurements.