Table 3.
Reaction Temp. (°C) |
Reaction Time (min) |
Heat of Crystallization (J/g) |
Heat of Fusion (J/g) |
Crystallization (%) |
---|---|---|---|---|
180 | 5 | −15.84 | 42.74 | 19.93 |
180 | 10 | −13.00 | 43.32 | 22.46 |
180 | 15 | 0 | 45.93 | 34.02 |
200 | 3 | −22.19 | 44.80 | 16.75 |
200 | 5 | −21.38 | 46.06 | 18.28 |
200 | 8 | 0 | 34.34 | 25.44 |
250 | 2 | −11.82 | 43.97 | 23.81 |
250 | 3 | −1.69 | 38.03 | 26.92 |
Before decomposition | −2.41 | 30.73 | 20.97 |