Table 4.
FR Treatment |
Flax/PP | Flax/PLA | ||||||||
---|---|---|---|---|---|---|---|---|---|---|
Mass Loss Stages | DTG Maxima (°C) | Char at 700 °C (%) | Mass Loss Stages | DTG Maxima (°C) | Char at 700 °C (%) | |||||
Stage | Temp Range (°C) | Mass Loss (%) | Stage | Temp Range (°C) | Mass Loss (%) | |||||
- | I | 219 *–380 | 87.8 | 341 | 0.3 | I | 252 *–388 | 91.1 | 358 | 0.8 |
II | 380–395 | 10.0 | 391 | II | 388–440 | 6.3 | 436 | |||
AS | I | 194 *–293 | 23.8 | 239 | 2.9 | I | 201 *–290 | 29.6 | 240 | 3.9 |
II | 293–385 | 48.6 | 368 | II | 290–412 | 40.6 | 356 | |||
III | 385–589 | 22.4 | 497 s | III | 412–565 | 22.2 | 463 s | |||
AB | I | 209 *–241 | 13.1 | 225 | 0.8 | I | 206 *–246 | 21.0 | 225 | 1.1 |
II | 241–412 | 64.2 | 384 | II | 246–405 | 55.4 | 349 | |||
III | 412–601 | 18.7 | 471 s | III | 405–590 | 18.5 | 458 (s) | |||
GDP | I | 200 *–276 | 22.2 | 261 | 5.1 | I | 199 *–290 | 21.5 | 273 | 7.6 |
II | 276–376 | 43.0 | 344 | II | 290–392 | 47.7 | 366 | |||
III | 376–633 | 26.1 | 537 s | III | 392–614 | 20.9 | 467 s | |||
GUP | I | 186 *–299 | 44.4 | 256 | 3.1 | I | 192 *–310 | 36.2 | 286 | 4.6 |
II | 299–381 | 19.8 | 324 | II | 310–393 | 35.1 | 351 | |||
III | 381–630 | 29.9 | 557 s | III | 393–623 | 21.3 | 475 s |
Note: * = Onset of decomposition temperature. There is small mass loss (~3%) from room temperature (RT) to the onset of decomposition temperature, corresponding to the volatilisation of moisture in the samples. s = represents small peak.