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. 2020 Nov 17;25(22):5373. doi: 10.3390/molecules25225373

Scheme 2.

Scheme 2

Synthesis of a coronene bisimide amphiphile using Diels–Alder cycloaddition to the bay region of perylene [126]. Reagents and conditions: (a) p-chloranil, 240 °C, 10 min, Y = 99%; (b) dodecylamine, DMF, rfx, 12 h, Y = 68%; (c) maleic anhydride, p-chloranil, 240 °C, 4 days, Y = not reported; and (d) glycolamine, DMF, rfx, 12 h, Y = 42%.