Table 1.
Bond Lengths (Å) | |||||||
---|---|---|---|---|---|---|---|
Bi1–O5 | 2.314(10) | Bi1–O7 | 2.697(9) | Bi2–O9 | 2.311(9) | Bi2–O14 ii | 2.539(9) |
Bi1–O1 | 2.332(9) | Bi1–O15 | 2.710(9) | Bi2–O15 | 2.433(9) | Bi2–N4 | 2.640(11) |
Bi1–N1 | 2.386(12) | Bi1–O8 | 2.829(10) | Bi2–O8 | 2.484(10) | Bi2–O14 | 2.650(10) |
Bi1–O13 | 2.443(9) | Bi1–O17 | 2.841(10) | Bi2–O6 i | 2.491(9) | Bi2–O16 | 2.842(10) |
Bi1–N2 | 2.521(12) | Bi2–N3 | 2.506(10) | ||||
Bond Angles (°) | |||||||
O1–Bi1–N2 | 74.3(4) | O5–Bi1–O7 | 141.6(3) | O15–Bi2–N3 | 117.4(4) | ||
O1–Bi1–N1 | 68.8(4) | O5–Bi1–O17 | 121.4(3) | O15–Bi2–N4 | 141.6(3) | ||
O1–Bi1–O5 | 131.9(3) | O13–Bi1–O15 | 72.8(3) | O15–Bi2–O9 | 77.2(3) | ||
O1–Bi1–O13 | 135.0(3) | O13–Bi1–O8 | 88.2(3) | O14–Bi2–O16 | 117.2(3) | ||
O1–Bi1–O15 | 143.0(3) | O13–Bi1–O7 | 77.9(3) | O14–Bi2–O6 i | 70.4(3) | ||
O1–Bi1–O8 | 88.8(3) | O13–Bi1–O17 | 140.9(3) | O14–Bi2–O14 ii | 71.6(3) | ||
O1–Bi1–O7 | 67.3(3) | O15–Bi1–O8 | 65.0(3) | O14–Bi2–N3 | 145.4(3) | ||
O1–Bi1–O17 | 71.9(3) | O15–Bi1–O7 | 106.3(3) | O14–Bi2–N4 | 111.2(3) | ||
N2–Bi1–N1 | 84.0(4) | O15–Bi1–O17 | 72.6(3) | O14–Bi2–O9 | 144.6(3) | ||
N2–Bi1–O5 | 66.1(3) | O8–Bi1–O7 | 47.9(3) | O16–Bi2–O6 i | 79.4(3) | ||
N2–Bi1–O13 | 130.9(3) | O8–Bi1–O17 | 60.9(3) | O16–Bi2–O14 ii | 138.5(3) | ||
N2–Bi1–O15 | 107.2(3) | O7–Bi1–O17 | 95.0(3) | O16–Bi2–N3 | 69.3(4) | ||
N2–Bi1–O8 | 137.8(3) | O8–Bi2–O15 | 74.5(3) | O16–Bi2–N4 | 131.2(3) | ||
N2–Bi1–O7 | 141.2(3) | O8–Bi2–O14 | 72.2(3) | O16–Bi2–O9 | 65.1(3) | ||
N2–Bi1–O17 | 77.1(4) | O8–Bi2–O16 | 115.1(3) | O6 i–Bi2–O14 ii | 65.4(3) | ||
N1–Bi1–O5 | 80.6(4) | O8–Bi2–O6 i | 142.4(3) | O6 i–Bi2–N4 | 78.3(4) | ||
N1–Bi1–O13 | 77.0(4) | O8–Bi2–O14 ii | 106.2(3) | O6 i–Bi2–N4 | 122.8(3) | ||
N1–Bi1–O15 | 147.6(3) | O8–Bi2–N3 | 138.0(6) | O6 i–Bi2–O9 | 138.6(3) | ||
N1–Bi1–O8 | 126.0(4) | O8–Bi2–N4 | 75.4(3) | O14 ii–Bi2–N3 | 82.5(5) | ||
N1–Bi1–O7 | 78.1(4) | O8–Bi2–O9 | 75.5(3) | O14 ii–Bi2–N4 | 61.7(3) | ||
N1–Bi1–O17 | 139.7(4) | O15–Bi2–O14 | 80.7(3) | O14 ii–Bi2–O9 | 132.0(3) | ||
O5–Bi1–O13 | 66.4(3) | O15–Bi2–O16 | 48.6(3) | N3–Bi2–N4 | 73.3(6) | ||
O5–Bi1–O15 | 76.8(3) | O15–Bi2–O6 i | 95.5(3) | N3–Bi2–O9 | 69.2(6) | ||
O5–Bi1–O8 | 139.1(3) | O15–Bi2–O14 ii | 150.7(3) | N4–Bi2–O9 | 73.3(3) |
Symmetry codes: i −x, 1 − y, 1 − z; ii 1 − x, 1 − y, 1 − z.