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. 2020 Nov 19;25(22):5428. doi: 10.3390/molecules25225428

Table 1.

Quantitative values as average (mean ± SD) determination of bioactive molecules in virgin olive oils (VOOs) of Picholine marocaine from five provinces studied. Results are expressed as mg.kg−1.

Compounds\Region (Provinces) Fes-Meknes (Taounate) Drâa-Tafilalet (Errachidia) Tanger-Tetouan-Al Hoceïma (Chefchaouen) Fes-Meknes (Taza) Beni Mellal-Khenifra (Beni Mellal)
α-tocopherol 100.4 ± 0.14 55.8 ± 0.10 55.3 ± 0.27 38.4 ± 0.10 39.9 ± 0.24
α-tocotrienol <LOQ <LOQ 2.92 ± 0.07 1.97 ± 0.05 7.60 ± 0.04
β-tocopherol 2.1 ± 0.07 1.9 ± 0.07 2.1 ± 0.06 1.6 ± 0.07 1.7 ± 0.05
γ-tocopherol 5.2 ± 0.06 4.2 ± 0.05 4.5 ± 0.08 4.1 ± 0.10 4.3 ± 0.06
δ-tocopherol <LOD <LOD <LOD <LOD <LOD
Tyrosol <LOD <LOD 300.6 ± 11.26 <LOD 186.2 ± 2.58
Hydroxytyrosol 6.4 ± 0.54 <LOD 40.0 ± 1.46 2.8 ± 0.15 4.6 ± 0.07
Caffeic acid <LOQ <LOD <LOD <LOD 3.5 ± 0.06
Ferulic acid <LOD 4.4 ± 0.43 3.9 ± 0.07 2.0 ± 0.03 0.8 ± 0.04
10-hydroxy-oleuropein aglycone a 25.4 ± 0.09 1.2 ± 0.18 65.7 ± 3.81 0.3 ± 0.00 1.4 ± 0.24
Oleocanthal a <LOD <LOD <LOQ <LOQ 0.8 ± 0.00
Luteolin <LOQ <LOQ 6.4 ± 0.19 7.8 ± 0.72 6.3 ± 0.13
Oleacein 3.1 ± 0.15 0.2 ± 0.02 33.3 ± 1.91 2.3 ± 0.01 3.5 ± 0.17
Apigenin <LOQ <LOQ <LOQ <LOQ 6.1 ± 0.00
Oleuropein aglycone a 231.3 ± 4.45 1.9 ± 0.00 198.3 ± 13.17 18.6 ± 0.00 20.6 ± 1.24
Luteolin glucoside 2.5 ± 0.03 1.1 ± 0.51 1.5 ± 0.03 3.9 ± 0.22 5.5 ± 1.79
Elenolic acid 31.3 ± 2.00 8.7 ± 0.81 85.6 ± 2.67 13.7 ± 0.26 19.6 ± 1.63
Ligstroside aglycone b 57.3 ± 2.92 0.7 ± 0.04 21.4 ± 0.39 1.2 ± 0.07 3.9 ± 0.19
Acidity% 1.3% 2.0% 2.0% 2.0% 1.1%
∑Vitamin E 107.6 * 61.9 64.8 46.1 53.5
∑Phenolic alcohols 6.4 <LOD 340.6 2.8 190.8
∑Phenolic acids 31.3 13.1 89.5 15.8 24.0
∑Secoiridoids 314.0 3.9 285.4 20.1 26.6
∑Flavonoids 2.5 1.1 7.9 11.7 18.0
∑Phenols 354.2 ** 18.1 723.4 ** 50.4 259.4 **

Quantitative determination carried out according to the following standard compounds: a oleuropein; b verbascoside; * values reported are above 90 mg kg−1 complying with Regulation 432/2012 of European Union [27]; ** values reported are above 250 mg kg−1 complying with the EU Health Claim [28].