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Controlled potential electrolysis measurements at 1.55 V vs. NHE for 600 s followed by 300 s at 0.20 V vs. NHE (a) and simultaneous electrochemical quartz microbalance measurements (b) of the buffer solution (black), 0.5 mM NiMeso (green), 1.0 mM NiMeso (blue) and 5.0 mM NiMeso (purple) in a 0.1 M pH 7.0 phosphate buffer using a gold working electrode.
