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Controlled potential electrolysis measurements at 1.60 V vs. NHE for 600 s followed by 300 s at 0.20 V vs. NHE (a) and simultaneous electrochemical quartz microbalance measurements (b) of the buffer solution (black) and 1.0 mM NiMeso (blue) in a 0.1 M pH 6.5 phosphate buffer using a gold working electrode.
