TABLE 2.
Crystallography data collection and refinement statistics
| Data collection | |
| Space group | C 1 2 1 |
| Unit cell dimensions | |
| a, b, c (Å) | 120.25, 42.84, 61.17 |
| α, β, γ (°) | 90.00, 110.23, 90.00 |
| Resolution (Å) | 34.92–1.63 |
| R merge (%) | 0.05 |
| I/σI | 2.24 (at 1.63Å) |
| Completeness (%) | 100.0 (34.92–1.63) |
| Redundancy | 3 |
| CC 1/2 | 0.976 (0.556) |
| Refinement | |
| Resolution (Å) | 34.92–1.63 |
| Number of unique reflections | 36,781 |
| Rwork (Rfree) | 0.232 (0.269) |
| Number of atoms | 2,350 |
| Wilson B (Å2) | 17.420 |
| Average refined B factors (Å2) | 2.823 |
| r.m.s. deviations | |
| Bond lengths (Å) | 0.0067 |
| Bond angles (°) | 0.93 |
| Ramachandran analysis | |
| Favored (%) | 96 |
| Allowed (%) | 3 |
| Outliers (%) | 1 |
Numbers in parenthesis refer to the outer resolution shell.