Table 1.

Data collection and refinement statistics

	p52_1–321	p52_121–514/p8	p52_121–514 (ano)
Data collection
Wavelength (Å)	0.97973	0.96770	0.97977
Spacegroup	P 31	P 21	P 1
Unit cell parameters
a, b, c (Å)	104.3, 104.3, 165.0	74.2, 86.0, 92.2	60.5, 83.2, 86.0
α, β, γ (°)	90, 90, 120	90, 94.9, 90	82.7, 80.0, 77.5
Resolution range (Å)	46.97–2.80	19.92–2.68	49.16–2.60
	(2.89–2.80)	(2.95–2.68)	(2.69–2.60)
Unique reflections	49 518 (4628)	17 307 (865)	48 667 (4455)
R merge (%)	16.2 (282.9)	28.0 (142.9)	20.1 (134.2)
R pim (%)	5.3 (90.1)	14.0 (71.5)	8.1 (53.9)
I/σI	10.7 (1.0)	5.7 (1.2)	9.4 (1.5)
CC (1/2)	0.997 (0.325)	0.983 (0.318)	0.995 (0.494)
Multiplicity	10.4 (10.8)	4.9 (4.8)	7.0 (7.1)
Completeness (%)
spherical	100.0 (100.0)	53.4 (10.8)	98.7 (98.0)
ellipsoidal	-	88.7 (49.5)	-
Refinement
Resolution range (Å)	46.97–2.80	19.92–2.68
Unique reflections	46 992	17 099
Number of atoms	8572	5606
R work (%)	18.6	21.6
R free (%)	20.9	24.0
Mean B-factor (Å2)	88.9	53.2
RMS deviations
Bond lengths (Å)	0.0054	0.008
Bond angles (°)	1.4375	0.95
Ramachandran statistics (%)
Favored	81.17	95.20
Allowed	15.96	3.93
Outliers	2.87	0.87

Values in parentheses correspond to highest resolution shell.