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. 2020 Aug 1;27(12):3559–3569. doi: 10.1016/j.sjbs.2020.07.028

Table 1.

Compounds found in B. disticha bulb solvent extracts. UI = Unidentified, Un = Unknown, a = Component/compound, b = Chemical formula, c = Retention time, d = Percentage composition, e = Quality assurance of GC/MS library.

Compounda ChemicalFormulab RTc %Compositiond
QAe
B. disticha Acetone B. disticha Ethanol B. disticha Chloroform
UI 4.561 0.35 35
UI 4.921 19 11
UI 5.185 0.57 35
2-Dodecene C12H24 21.147 0.05 96
2-Methoxyl-4-vinylphenol C9H10O2 26.176 0.45 95
1-Tetradecene C14H28 29.212 0.16 2.15 98
Ethanone, 1-(4-hydroxy-3,5-dimethoxyphenyl)- C10H12O4 31.705 0.21 0.36 49
Apocynin (Powerful antioxidant) C9H10O3 33.054 21.80 15.53 1.08 97
2,4-Di-tert-butylphenol C14H22O 34.066 1.62 7.58 97
2-Tetradecene C14H28 37.126 0.58 3.35 99
Cyclohexadecane C16H32 37.126 0.58 3.35 94
4-octyldodecyl cyclopentane C25H50 37.461 0.2 60
UI 37.756 0.21 46
6-methyl-5-(1-methylethyl) 5-hepten-3-yn-2-ol C11H18O 41.144 0.01 55
Pyrimidine, 4,5-diamino-6-methoxy-meta-methoxybenzenethiol Un 42.859 0.43 64
7-Methyl-4-azafluorene C13H11N 43.126 0.03 50
UI 43.202 0.01 47
1-Octadecene CH3(CH2)15CH = CH2 44.337 0.79 3.97 99
Heptadecyl heptafluorobutyrate C21H35F7O2 44.604 0.18 51
Isophthalic acid, dodecyl methyl ester C21H32O4 44.740 0.01 60
UI 44.796 0.01 47
6,10,14-Trimethyl-pentadecan-2-ol C18H38O 46.116 0.10 89
4-(Methylthio)phenyl isothiocyanat C8H7NS2 46.224 0.17 50
1,2-Dimethoxy-4-(1,2,3-trimethoxyp ropyl)benzene Un 46.260 0.15 53
UI 46.589 0.17 49
7-Bromo-3a,6,6-trimethyl-hexahydro -benzofuran-2(3H)-one Un 46.658 0.1 55
UI 46.701 0.08 47
UI 46.761 0.15 47
Furane-3-carboxylic acid, 5-tert-b utyl-2-(4-tert-butylphenoxymethyl) Un 46.923 0.09 50
7-Bromo-3a,6,6-trimethyl-hexahydro -benzofuran-2(3H)-one Un 46.957 0.08 55
Furane-3-carboxylic acid, 5-tert-b utyl-2-(4-tert-butylphenoxymethyl) Un 47.244 0.25 50
Formaldehyde, O-[(pentafluoropheny l)methyl]oxime C8H4F5NO 47.329 0.09 50
UI 47.833 1.69 47
3-Fluoro-p-anisidine FC6H3(OCH3)NH2 47.836 1.16 50
Furane-3-carboxylic acid, 5-tert-b utyl-2-(4-tert-butylphenoxymethyl) Un 48.063 0.29 50
UI 48.100 0.57 49
UI 48.481 1.04 50
UI 48.624 0.13 49
Desmedipham C16H16N2O4 48.650 0.17 50
UI 49.001 0.15 30
UI 49.753 12.21 46
3,6-Dipropyl-1,2-dihydro-1,2,4,5-t etrazine Un 49.784 10.66 50
3,6-Dipropyl-1,2-dihydro-1,2,4,5-tetrazine Un 49.884 40.32 53
n-Hexadecanoic acid C16H32O2 50.079 3.13 0.56 99
UI 50.259 0.18 43
Trifluoroacetoxy hexadecane C18H33F3O2 50.892 1.03 94
1-Nonadecene C19H3 50.917 4.30 94
UI 51.937 0.03 35
UI 52.257 0.06 38
UI 52.332 0.03 42
UI 52.836 0.63 45
UI 53.691 0.84 45
Hexadecane C16H34 54.176 0.10 70
Phytol C20H40O 54.533 0.15 99
9,12-Octadecadienoic acid (z,z) C18H32O2 55.227 2.32 0.27 99
Z,E-2,13-octadecadien-1-ol C18H34O 55.238 0.28 90
(z)-18-Octadec-9-enolide C18H32O2 55.246 0.46 99
UI 55.396 0.51 46
(1aR,4s,4aR,7R,7aS,7bS)-1,1,4,7-Tetramethyldecahydro-1H-cyclopropa[e]azulen-4-ol C15H26O 55.681 0.07 90
Z,z-10,12-Hexadecadien-1-ol acetate C18H32O2 55.711 0.08 80
2-(3-Hydroxylbutyl) cyclooctanone C12H22O2 55.742 0.05 64
Octadecanoic acid C17H35CO2H 56.142 0.61 96
2-hydroxyl-cyclopentadecanone C15H28O2 56.769 0.24 90
2-Dodecen-1-yl(-)succinic anhydrid C16H26O3 56.782 0.11 58
9-Nonadecene C19H38 56.903 0.67 91
Heptadecyl triflouroacetate C19H35F3O2 56.937 3.35 94
4-Octyldodecyl cyclopentane C25H50 57.083 0.68 93
Benzaldehyde, 4-[1-[4-(acetyloxy)- 3,5-dimethoxyphenyl]ethoxy]-3-methoxy Un 57.870 1.56 62
Dodecyl methyl ester Isophthalic acid C21H32O4 57.902 2.09 68
4-(4-Methylaminobenzylideneamino)benzonitrile Un 58.050 0.34 53
UI 58.977 1.61 43
UI 59.542 12.08 49
UI 59.897 1.18 44
Dodecyl phthalate C20H30O4 60.209 2.21 95
Undulatine C18H21NO5 61.021 2.38 99
UI 61.059 0.08 35
UI 61.086 0.03 35
UI 61.119 0.03 45
1,2-Benzenedicarboxylic acid, bis(8-methylnonyl) ester Un 61.253 1.8 98
UI 61.261 2.26 38
2,2 dimethyl-6-methylene cyclohexanepropanol C12H22O 61.387 1.10 59
UI 61.631 0.33 35
UI 61.786 1.64 41
1,2-Benzenedicarboxylic acid Bis (8-methylnonyl) ester Un 61.776 2.33 98
UI 61.810 0.35 42
UI 62.138 6.16 53
Ethyl-cyclodocosane C24H48 62.426 0.82 95
Cyclotetracosane C24H48 62.444 2.25 96
Epibuphanisine C17H19NO3 62.571 2.31 6.16 5.92 99
2,3,5,6-Tetramethyl-para-phenylenediamine (CH3)4C6(NH2)2 62.896 0.87 58
UI 63.269 0.67 47
Silane, diethylisohexyloxy(1-naphthydoxy)- Un 63.298 0.65 64
1,2-Benzenedicarboxylic acid, bis(8-methylnonyl) ester Un 63.583 1.14 98
UI 63.913 2.61 25
UI 63.966 0.63 43
UI 64.006 2.29 15
UI 64.314 0.37 46
Bis (8-methylnonyl) ester 1,2-Benzenedicarboxylic acid Un 65.046 0.64 1.06 98
Eicosane C20H42 65.189 0.27 89
Benzenemethanol, 4-(1,1-dimethylethyl)- C11H16O 65.287 0.19 58
UI 65.350 0.22 47
Buphandrin C18H21NO4 65.554 −3.27 1.06 −2.05 99
Guaia-9–11-diene C15H24 65.606 0.22 55
1,3-bis([(2Z)-3,7-Dimethylocta-2,6-dien-1-yl]oxy)-1,1,3,3-tetramethyldisiloxane C24H46O3Si2 65.689 0.18 90
Alloaromadendrene C15H24 65.730 0.09 59
Alpha-Cadinol C15H26O 65.845 0.47 53
UI 65.930 0.4 43
1,2-Benzenedicarboxylic acid, bis(8-methylnonyl) ester Un 66.615 0.17 1.06 98
Buphandrin C18H21NO4 67.561 −3.27 1.06 −2.05 99
%Total content 94.3 59.28 84.02

(–) denote no detection.