Table 1.
X-ray diffraction data processing and refinement statistics.
| Statistic Value for: | cCD8αα/pBF2*0401 | cCD8αα/pBF2*1501 | BF2*1501/RY0808 |
|---|---|---|---|
| Data processing | |||
| Space group | P21 | P1 | P3121 |
| Cell parameters | |||
| a (Å) | 90.576 | 51.34 | 123.45 |
| b (Å) | 90.82 | 66.73 | 123.45 |
| c (Å) | 94.87 | 103.95 | 81.22 |
| α (°) | 90.00 | 84.60 | 90.00 |
| β (°) | 98.61 | 82.04 | 90.00 |
| γ (°) | 90.00 | 67.51 | 120.00 |
| Resolution range (Å) | 50.00-2.80(2. 90–2.80) | 50.00-2.6(2.69–2.6) | 50.00-2.71(2.77–2.71) |
| Total reflections | 163307 | 108500 | 111237 |
| Unique reflections | 37565 | 36586 | 18044 |
| Completeness (%) | 99.57 (97.75) | 95.34 (93.09) | 96.2(97.7) |
| Redundancy | 4.3(4.5) | 3.0(3.1) | 3.4(2.1) |
| Rmerge (%) | 10.5(61.3) | 10.9(51.6) | 8.0(24.00) |
| I/σ (I) | 10.21 (3.04) | 8.25 (3.24) | 11.09(2.659) |
| Refinement | |||
| Rwork | 0.2519 | 0.2533 | 0.2304 |
| Rfree | 0.2881 | 0.2990 | 0.2647 |
| RMSD | |||
| Bond lengths (Å) | 0.005 | 0.010 | 0.004 |
| Bond angles (°) | 1.16 | 1.68 | 0.865 |
| Average B factor | 80.60 | 58.40 | 59.58 |
| Ramachandran plot | |||
| Most favored (%) | 97 | 96 | 97.1 |
| Disallowed (%) | 0.17 | 0 | 0 |