Table 2.
MW #1 | MW #2 Small Agglomerates |
MW #2 Large Agglomerates |
MW #3 | MW #4 | MW #5 | MW #6 | MW #7 | CNF #1 | CNF #2 | |
---|---|---|---|---|---|---|---|---|---|---|
Spherical Agglomerates | ||||||||||
% Spherical Agglomerated | 87 | 0 | 0 | 83 | 1 | 4 | 0 | 0 | 0 | 0 |
Spherical Agglomerate Mean Diameter μm ± SE |
1.28 ± 0.16 | N/A | N/A | 0.81 ± 0.10 | N/A | N/A | N/A | N/A | N/A | N/A |
Spherical Agglomerate Diameter Geometric Mean μm (GSD) |
0.96 (2.01) | N/A | N/A | 0.66 (1.84) | N/A | N/A | N/A | N/A | N/A | N/A |
Bundled Agglomerates | ||||||||||
% Bundle Agglomerates/Singlets | 13 | N/A | N/A | 17 | 99 | 96 | 100 | 100 | 100 | 100 |
Bundle Agglomerate Mean Length μm ± SE |
1.90 ± 0.37 | 3.80 ± 0.38 | 49.55 ± 3.58 | 1.11 ± 0.25 | 3.77 ± 0.35 | 6.27 ± 0.44 | 9.47 ± 1.26 | 11.32 ± 1.08 | 9.30 ± 1.07 | 2.96 ± 0.36 |
Bundle Agglomerate Geometric Mean Length μm (GSD) |
1.66 (1.71) | 3.09 (1.82) | 47.94 (1.31) | 0.72 (2.98) | 2.92 (2.05) | 5.17 (1.94) | 5.90 (2.57) | 7.91 (2.49) | 6.18 (2.49) | 2.11 (2.25) |
Bundle Agglomerate Mean Diameter μm ± SE |
0.38 ± 0.12 | 0.03 ± 0.00 | 9.50 ± 2.24 | 0.03 ± 0.00 | 0.10 ± 0.01 | 0.13 ± 0.01 | 0.08 ± 0.01 | 0.10 ± 0.01 | 0.21 ± 0.01 | 0.12 ± 0.01 |
Bundle Agglomerate Diameter Geometric Mean μm (GSD) |
0.18 (4.20) | 0.03 (1.60) | 6.99 (2.24) | 0.03 (1.56) | 0.08 (1.89) | 0.11 (1.07) | 0.07 (2.09) | 0.09 (1.64) | 0.19 (1.42) | 0.11 (1.63) |
Hydrodynamic Diameter (nm) |
660 ± 19 | 771 ± 33 | 608 ± 30 | 478 ± 24 | 504 ± 15 | 714 ± 24 | 652 ± 26 | 615 ± 19 | 664 ± 18 | |
Zeta Potential (pH 7.3) | −10.4 ± 0.4 | −12.1 ± 0.6 | −11.1 ± 0.06 | −12.0 ± 0.4 | −13.5 ± 0.8 | −11.8 ± 0.6 | −13.2 ± 0.5 | −11.1 ± 0.8 | −11.3 ± 0.5 |