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. 2020 May 6;142(22):10198–10211. doi: 10.1021/jacs.0c03577

Figure 2.

Figure 2

Thermal stability and decomposition of Pb4S3Br2 NCs. (a) TGA curve of a Pb4S3Br2 NC sample, showing the three distinct weight losses that the material undergoes upon heating. (b) Rietveld fit of the product of the first mass loss (∼350 °C), demonstrating that what is left after this step is a mixture of PbS and Pb7S2Br10. (c) Rietveld fit of the XRPD pattern for the product of the second mass loss (∼600 °C), demonstrating that only PbS is left.