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. 2020 Dec 8;5(50):32515–32529. doi: 10.1021/acsomega.0c04706

Table 4. Cyclocarbonylative Sonogashira Coupling Reactions of 4′-Hydroxy-3′-iodoaryls (1a–d) with Alkyl Alkynes (5a–e) Catalyzed by C1a.

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a

Reaction conditions: C1 (1.0 mol %), 4′-hydroxy, 3′-iodoaryl (0.50 mmol), alkyl alkyne (0.60 mmol), Et2NH (1.0 mmol), DMF (2.5 mL), CO (100 psi), 110 °C, 24 h.

b

Isolated yield.