Table 1.
HS-SPME-GC-MS degradation relating retention time to its IUPAC name.
| Retention Time (min) |
Compound Name (IUPAC Name) | H2SO4 v HCl 1 | H2SO4 v NaOH 1 |
|---|---|---|---|
| 16.53 | dihydroxy(dimethyl)silane | - | <0.01 |
| 16.93 | 2,2,4,4,6,6-hexamethyl-1,3,5,2,4,6-trioxatrisilinane | <0.01 | >0.01 |
| 23.1 | 2,2,4,4,6,6,8,8-octamethyl-1,3,5,7,2,4,6,8-tetraoxatetrasilocane | <0.01 | >0.01 |
| 24.03 | [(dimethyl-3-silanyl)oxy-dimethylsilyl]oxy-dimethylsilicon | <0.01 | - |
| 24.3 | trimethoxy(methyl)silane | - | - |
| 28.51 | 2-Hydroxymandelic acid, ethyl ester, di-TMS | >0.01 | >0.01 |
| 28.51_2 | 2,4-bis(trimethylsilyloxy)benzaldehyde | <0.01 | <0.01 |
| 28.53 | Tetramethylsilane | <0.01 | <0.01 |
| 29.28 | 2,2,4,4,6,6-hexamethyl-1,3,5,2,4,6-trioxatrisilinane | - | <0.01 |
| 33.87 | Tetramethylsilane | >0.01 | >0.01 |
| 36.56 | trimethyl(1-trimethylsilylethyl)silane | >0.01 | - |
| 38.75 | bis[[dimethyl(trimethylsilyloxy)silyl]oxy]-dimethylsilane | <0.01 | <0.01 |
1 Wilcoxon-signed rank test (p-value).