Skip to main content
. 2020 Dec 11;25(24):5866. doi: 10.3390/molecules25245866

Table 3.

Limit of quantitation (LOQ), linearity of calibration (r2), recovery, and matrix effect validation results for the 353 target pesticides.

No. Compound Name LOQ
(μg/kg)
r2 Linear
Range
(μg/kg)
Recovery ME 2
(%)
Low High
Conc. 1
(μg/kg)
Value
(%)
RSD
(%)
Conc.
(μg/kg)
Value
(%)
RSD
(%)
1 Abamectin 10 0.9923 10–200 10 108.1 13.9 50 112.5 8.3 11.8
2 Acetamiprid 1 0.9975 1–200 1 90.2 12.2 50 103.8 3.2 5.8
3 Acibenzolar-S-methyl 5 0.9991 5–200 5 100.5 15.8 50 83.3 4.8 4.9
4 Alachlor 5 0.9993 5–200 5 90.2 14.1 50 93.5 2.7 −6.8
5 Aldicarb sulfone 1 0.9993 1–200 1 87.4 18.7 50 101.5 2.0 −0.7
6 Aldicarb sulfoxide 1 0.9999 1–200 1 82.8 12.2 50 94.7 1.4 −11.3
7 Allethrin 10 0.9971 10–200 10 85.5 13.2 50 84.7 3.2 −9.2
8 Ametoctradin 2.5 0.9996 2.5–200 2.5 80.4 8.9 50 80.5 3.2 −4.7
9 Ametryn 10 0.9982 10–200 10 65.8 4.4 50 75.0 7.1 −6.5
10 Anilofos 1 0.9980 1–200 1 102.9 16.5 50 94.2 10.2 −6.5
11 Aramite 1 0.9997 1–200 1 89.1 15.9 50 94.4 4.7 −24.0
12 Aspon 1 0.9998 1–200 1 87.7 4.2 50 89.5 1.9 −10.6
13 Atrazine 1 0.9999 1–200 1 89.5 6.6 50 85.6 1.2 1.9
14 Azaconazole 1 0.9983 1–200 1 76.9 8.3 50 87.6 3.5 5.3
15 Azimsulfuron 2.5 0.9992 2.5–200 2.5 84.9 14.1 50 92.8 4.2 2.9
16 Azinphos-ethyl 2.5 0.9925 2.5–200 2.5 106.2 8.6 50 113.7 9.8 −21.3
17 Azinphos-methyl 2.5 0.9931 2.5–200 2.5 95.3 14.5 50 107.8 8.1 −17.8
18 Azoxystrobin 1 0.9950 1–200 1 93.5 9.8 50 105.6 3.6 −2.6
19 Benalaxyl 1 0.9980 1–200 1 91.5 11.3 50 97.5 5.1 −13.5
20 Bendiocarb 2.5 0.9982 2.5–200 2.5 95.4 5.8 50 95.4 4.5 3.3
21 Benodanil 1 0.9997 1–200 1 92.4 7.3 50 96.8 2.8 1.7
22 Benoxacor 2.5 0.9988 2.5–200 2.5 96.7 14.8 50 96.6 3.8 3.2
23 Bensulfuron-methyl 1 0.9994 1–200 1 88.7 15.6 50 94.6 4.5 7.7
24 Bensulide 2.5 0.9942 2.5–200 2.5 73.0 16.4 50 111.4 6.9 −22.6
25 Benthiavalicarb-isopropyl 1 0.9994 1–200 1 107.1 11.8 50 95.6 2.7 1.8
26 Benzobicyclon 1 0.9993 1–200 1 118.0 9.1 50 94.6 3.4 15.6
27 Benzoximate 5 0.9959 5–200 5 69.1 9.5 50 87.5 9.3 −6.9
28 Benzoylprop-ethyl 2.5 0.9997 2.5–200 2.5 103.7 8.7 50 96.3 7.2 −4.5
29 Bitertanol 5 0.9976 5–200 5 96.4 13.3 50 95.7 7.2 10.4
30 Bixafen 1 0.9974 1–200 1 109.6 18.1 50 97.1 9.4 −8.0
31 Boscalid 5 0.9992 5–200 5 89.0 7.3 50 96.1 3.1 5.6
32 Broflanilide 10 0.9965 10–200 10 111.6 16.9 50 103.7 5.7 11.5
33 Broflanilide_DM-8007 1 0.9994 1–200 1 114.8 14.9 50 97.1 6.9 −0.2
34 Broflanilide_S(PFP-OH)-8007 10 0.9977 10–200 10 97.6 14.5 50 106.1 7.6 −4.7
35 Bromacil 2.5 0.9978 2.5–200 2.5 91.6 9.4 50 96.7 5.2 4.4
36 Bromobutide 2.5 0.9983 2.5–200 2.5 99.1 15.8 50 99.0 9.2 −7.1
37 Bromuconazole 5 0.9977 5–200 5 78.1 12.5 50 85.2 7.9 6.1
38 Bupirimate 1 0.9969 1–200 1 86.5 18.1 50 91.4 10.7 −3.4
39 Buprofezin 2.5 0.9998 2.5–200 2.5 73.2 8.5 50 72.1 6.4 −26.5
40 Butocarboxim 10 0.9958 10–200 10 116.8 8.4 50 106.4 6.9 −4.5
41 Cadusafos 1 0.9989 1–200 1 73.5 6.8 50 88.1 2.0 2.8
42 Cafenstrole 2.5 0.9997 2.5–200 2.5 99.2 13.1 50 106.7 8.6 0.4
43 Carbaryl 1 0.9988 1–200 1 83.3 19.2 50 89.8 4.3 4.1
44 Carbendazim 1 0.9999 1–25 1 46.6 14.7 10 47.5 6.6 −2.3
45 Carbetamide 2.5 0.9958 2.5–200 2.5 75.2 10.0 50 95.4 5.0 12.6
46 Carbofuran 10 0.9902 10–200 10 79.4 7.3 50 115.6 4.7 −25.4
47 Carbofuran-3-hydroxy 5 0.9989 5–200 5 84.7 17.8 50 95.6 8.3 10.5
48 Carboxin 1 0.9986 1–200 1 88.9 11.4 50 88.3 3.4 −8.6
49 Carfentrazone-ethyl 10 0.9994 10–200 10 91.8 19.9 50 93.6 4.7 1.0
50 Carpropamid 5 0.9976 5–200 5 86.9 14.8 50 98.4 3.7 −1.4
51 Chlorantraniliprole 1 0.9994 1–200 1 100.6 17.1 50 96.8 4.2 9.1
52 Chlorbenzuron 10 0.9950 10–200 10 84.9 19.7 50 95.0 9.1 5.6
53 Chlorfenvinphos 2.5 0.9989 2.5–200 2.5 90.3 8.0 50 96.0 6.2 −18.2
54 Chlorimuron-ethyl 1 0.9995 1–200 1 89.8 11.1 50 92.3 3.5 8.4
55 Chlorotoluron 1 0.9998 1–200 1 94.3 8.5 50 92.7 3.2 −7.2
56 Chloroxuron 1 0.9966 1–200 1 103.3 16.9 50 97.0 6.8 −2.1
57 Chlorpyrifos 2.5 0.9997 2.5–200 2.5 86.6 12.8 50 83.9 3.9 −14.9
58 Chlorsulfuron 5 0.9965 5–200 5 61.5 10.9 50 88.9 15.9 −2.4
59 Chromafenozide 1 0.9970 1–200 1 96.5 9.7 50 97.3 8.1 −2.0
60 Clethodim 1 0.9975 1–200 1 93.8 19.2 50 82.3 7.1 2.1
61 Clofentezine 1 0.9985 1–200 1 64.9 18.1 50 55.0 7.9 4.7
62 Clomazone 2.5 0.9980 2.5–200 2.5 94.1 8.0 50 91.4 5.0 14.7
63 Clothianidin 5 0.9979 5–200 5 83.3 14.3 50 88.8 7.1 9.5
64 Coumaphos 1 0.9982 1–200 1 82.1 8.4 50 92.5 2.7 4.6
65 Crotoxyphos 10 0.9991 10–200 10 42.9 11.4 50 68.2 8.5 2.6
66 Crufomate 2.5 0.9989 2.5–200 2.5 92.3 5.2 50 98.0 4.9 −9.7
67 Cyanazine 2.5 0.9993 2.5–200 2.5 100.1 11.1 50 99.1 4.1 10.5
68 Cyazofamid 1 0.9978 1–200 1 99.3 7.3 50 97.7 4.4 8.8
69 Cyclosulfamuron 1 0.9950 1–200 1 92.1 15.6 50 100.5 2.7 −2.8
70 Cyflufenamid 1 0.9966 1–200 1 100.5 18.8 50 103.6 3.2 −14.3
71 Cyhalofop-butyl 10 0.9980 10–200 10 90.9 11.1 50 90.2 13.3 8.5
72 Cymoxanil 2.5 0.9988 2.5–200 2.5 89.0 13.0 50 94.9 5.3 13.0
73 Cyprazine 1 0.9998 1–200 1 95.2 6.3 50 86.6 4.2 −3.3
74 Cyprodinil 10 0.9995 10–200 10 43.5 7.1 50 55.2 5.7 −4.1
75 Daimuron 1 0.9993 1–200 1 83.5 11.3 50 97.2 4.4 7.9
76 Demeton-S 1 0.9961 1–200 1 91.3 13.3 50 99.6 6.6 5.7
77 Demeton-S-methyl 5 0.9976 5–200 5 81.2 9.3 50 98.6 8.3 8.9
78 Demeton-S-methyl sulfone 2.5 0.9987 2.5–200 2.5 71.2 11.0 50 94.5 7.0 7.5
79 Demeton-S-methyl sulfoxide 2.5 0.9995 2.5–200 2.5 79.9 7.9 50 87.5 3.8 −1.2
80 Desmetryn 10 0.9990 10–200 10 70.1 3.4 50 74.0 2.7 0.8
81 Diazinon 2.5 0.9993 2.5–200 2.5 89.3 10.4 50 88.4 3.7 −3.2
82 Diclobutrazol 10 0.9987 10–200 10 86.6 7.0 50 88.2 6.5 −9.1
83 Dicrotophos 5 0.9999 5–200 5 52.6 18.4 50 73.8 8.7 −0.2
84 Diethatyl-ethyl 1 0.9992 1–200 1 107.5 9.8 50 97.8 7.2 0.7
85 Diethofencarb 1 0.9993 1–200 1 111.9 10.9 50 97.6 5.2 16.6
86 Difenoconazole 1 0.9996 1–200 1 108.5 17.4 50 88.5 2.1 −1.7
87 Diflubenzuron 1 0.9993 1–200 1 103.9 18.7 50 98.5 4.5 2.6
88 Diflufenican 1 0.9996 1–200 1 86.3 11.9 50 94.1 3.6 10.1
89 Dimepiperate 5 0.9937 5–200 5 97.1 9.1 50 91.1 11.5 −9.7
90 Dimethachlor 2.5 0.9996 2.5–200 2.5 91.2 14.4 50 97.6 2.6 1.9
91 Dimethametryn 1 0.9990 1–200 1 62.0 8.6 50 69.1 3.6 −2.9
92 Dimethenamide 2.5 0.9987 2.5–200 2.5 83.2 10.8 50 96.1 3.2 −1.7
93 Dimethoate 1 0.9979 1–200 1 98.3 16.7 50 100.4 7.3 4.4
94 Dimethomorph 1 0.9993 1–200 1 95.1 18.7 50 101.2 2.4 7.5
95 Dimethylaminosulfotoluidide (DMST) 1 0.9989 1–25 1 94.2 15.3 10 88.9 4.7 6.0
96 Dimethylvinphos (E) 2.5 0.9989 2.5–200 2.5 100.6 15.7 50 95.9 6.0 2.3
97 Dimethylvinphos (Z) 10 0.9996 10–200 10 63.3 6.2 50 84.0 4.3 −0.2
98 Diniconazole 5 0.9997 5–200 5 57.0 16.7 50 90.6 4.2 −19.3
99 Dinotefuran 5 0.9987 5–200 5 104.8 16.4 50 103.1 5.8 −21.9
100 Diphenamid 1 0.9958 1–200 1 86.0 6.2 50 103.8 3.7 0.7
101 Dithiopyr 1 0.9997 1–200 1 86.5 12.3 50 98.2 3.7 4.8
102 Diuron 1 0.9996 1–200 1 94.2 11.6 50 92.2 3.0 4.5
103 Edifenphos 10 0.9932 10–200 10 71.4 6.3 50 85.7 7.9 −6.9
104 Esprocarb 2.5 0.9992 2.5–200 2.5 83.4 10.3 50 83.1 5.9 −24.4
105 Etaconazole 2.5 0.9981 2.5–200 2.5 92.5 18.1 50 94.6 5.0 −4.1
106 Ethaboxam 2.5 0.9978 2.5–200 2.5 119.8 7.3 50 99.7 2.1 12.0
107 Ethiofencarb 1 0.9992 1–200 1 92.3 15.4 50 93.6 5.1 3.3
108 Ethoprophos 1 0.9933 1–200 1 83.7 16.1 50 100.6 6.3 0.2
109 Ethoxysulfuron 2.5 0.9973 2.5–200 2.5 76.3 14.8 50 87.9 4.4 −10.4
110 Etofenprox 1 0.9996 1–200 1 81.5 13.3 50 75.2 1.4 −10.8
111 Etoxazole 1 0.9968 1–200 1 74.9 2.3 50 88.9 2.0 −12.5
112 Etrimfos 2.5 0.9994 2.5–200 2.5 95.0 11.7 50 94.8 3.7 −4.3
113 Famoxadone 5 0.9959 5–200 5 95.4 18.7 50 102.7 5.6 0.4
114 Fenamiphos 1 0.9997 1–200 1 97.8 13.4 50 93.0 6.1 −1.7
115 Fenamiphos sulfone 2.5 0.9949 2.5–200 2.5 102.9 19.6 50 86.4 7.4 6.5
116 Fenamiphos sulfoxide 1 0.9994 1–200 1 79.9 15.1 50 85.1 5.3 12.3
117 Fenazaquin 1 0.9999 1–200 1 57.2 8.3 50 61.2 2.8 –39.7
118 Fenbuconazole 2.5 0.9979 2.5–200 2.5 95.9 17.0 50 98.4 5.8 2.2
119 Fenfuram 1 0.9982 1–200 1 89.8 14.3 50 105.1 4.6 –2.1
120 Fenhexamid 10 0.9991 10–200 10 71.3 12.7 50 93.1 5.1 5.8
121 Fenobucarb 1 0.9997 1–200 1 94.0 7.2 50 92.8 5.1 –3.2
122 Fenothiocarb 1 0.9996 1–200 1 100.4 15.0 50 92.8 2.7 –0.1
123 Fenoxanil 2.5 0.9994 2.5–200 2.5 108.5 17.4 50 97.1 5.0 –1.1
124 Fenoxaprop-ethyl 1 0.9988 1–200 1 84.8 7.6 50 91.4 3.7 1.0
125 Fenoxycarb 5 0.9996 5–200 5 87.4 7.5 50 100.5 5.9 –1.6
126 Fenpropathrin 1 0.9997 1–200 1 71.4 15.8 50 90.7 2.7 13.6
127 Fenpropimorph 1 0.9989 1–200 1 88.6 16.3 50 83.6 5.6 –0.4
128 Fenpyroximate 1 0.9999 1–200 1 84.0 6.3 50 85.0 1.4 16.4
129 Fenquinotrione 10 0.9998 10–200 10 47.3 18.6 50 49.7 8.1 7.3
130 Fenthion 2.5 0.9972 2.5–200 2.5 75.7 12.3 50 91.6 4.0 2.3
131 Fenthion oxon 1 0.9977 1–200 1 97.2 2.9 50 93.0 4.5 2.7
132 Fenthion oxon sulfoxide 2.5 0.9994 2.5–200 2.5 73.5 15.8 50 81.3 2.4 3.2
133 Fenthion sulfone 1 0.9974 1–200 1 105.9 19.2 50 101.6 3.6 17.8
134 Fenthion sulfoxide 1 0.9988 1–200 1 72.5 19.5 50 100.1 5.0 4.3
135 Fentrazamide 1 0.9980 1–200 1 103.2 11.8 50 99.2 8.3 12.4
136 Ferimzone 5 0.9991 5–200 5 41.0 18.3 50 67.0 1.4 –1.9
137 Fipronil 1 0.9995 1–200 1 99.9 5.1 50 97.8 1.2 24.7
138 Fipronil sulfone 1 0.9998 1–200 1 97.2 3.5 50 100.7 2.8 4.8
139 Flamprop-isopropyl 1 0.9989 1–200 1 89.8 16.0 50 99.9 5.8 –1.3
140 Flonicamid 2.5 0.9982 2.5–200 2.5 89.6 12.0 50 100.3 5.0 –11.2
141 Fluacrypyrim 1 0.9983 1–200 1 85.1 18.9 50 99.9 6.6 –9.6
142 Fluazinam 1 0.9999 1–200 1 80.3 2.5 50 86.1 0.8 12.8
143 Flucetosulfuron 10 0.9957 10–200 10 59.0 8.9 50 75.2 6.9 0.7
144 Fludioxonil 1 0.9997 1–200 1 90.4 8.1 50 95.3 2.9 16.5
145 Flufenacet 1 0.9944 1–200 1 101.3 11.2 50 105.6 10.9 1.8
146 Flufenoxuron 1 0.9999 1–200 1 88.9 5.8 50 93.0 3.9 11.0
147 Fluometuron 5 0.9994 5–200 5 87.2 19.4 50 96.2 3.9 5.5
148 Fluopicolide 1 0.9974 1–200 1 86.7 9.7 50 99.0 3.4 3.6
149 Fluopyram 1 0.9983 1–200 1 99.6 11.5 50 101.7 9.0 –0.3
150 Flupyradifuron 1 0.9944 1–200 1 95.6 16.0 50 104.2 3.2 9.9
151 Fluquinconazole 2.5 0.9983 2.5–200 2.5 101.8 14.9 50 93.0 4.0 –4.5
152 Fluridone 1 0.9982 1–200 1 86.5 9.6 50 98.6 6.9 –3.1
153 Flurochloridone 2.5 0.9940 2.5–200 2.5 88.5 17.6 50 96.8 7.9 1.0
154 Flurtamone 1 0.9932 1–200 1 98.7 11.0 50 101.6 7.7 –4.2
155 Flusilazole 1 0.9994 1–200 1 92.8 17.2 50 92.7 5.5 –8.6
156 Fluthiacet-methyl 10 0.9964 10–200 10 71.6 12.4 50 76.7 15.6 6.6
157 Flutianil 1 0.9983 1–200 1 95.7 15.3 50 95.7 5.2 5.6
158 Flutolanil 1 0.9943 1–200 1 90.8 11.1 50 102.2 4.8 –0.8
159 Flutriafol 1 0.9990 1–200 1 101.2 13.0 50 98.0 3.8 –0.4
160 Fluxapyroxad 1 0.9977 1–200 1 97.3 12.6 50 104.5 4.7 –5.3
161 Forchlorfenuron 1 0.9979 1–200 1 81.0 17.3 50 87.9 3.0 2.6
162 Fosthiazate 1 0.9979 1–200 1 88.0 7.8 50 99.6 1.9 –1.5
163 Halosulfuron-methyl 2.5 0.9959 2.5–200 2.5 88.1 13.9 50 90.4 8.7 –2.7
164 Haloxyfop 2.5 0.9991 2.5–200 2.5 94.8 11.5 50 84.9 2.9 11.4
165 Heptenophos 10 0.9997 10–200 10 69.0 5.2 50 83.8 5.4 –7.2
166 Hexaconazole 10 0.9954 10–200 10 80.6 12.6 50 87.6 3.3 –14.8
167 Hexazinone 1 0.9948 1–200 1 77.8 8.6 50 99.7 6.9 1.1
168 Hexythiazox 1 0.9990 1–200 1 81.5 17.9 50 80.6 3.1 –0.4
169 Imazalil 5 0.9997 5–200 5 78.1 7.0 50 87.7 2.6 –15.8
170 Imazamox 10 0.9988 10–200 10 62.9 7.9 50 68.2 6.4 8.3
171 Imazapic 2.5 0.9987 2.5–200 2.5 72.5 7.2 50 69.1 3.6 5.3
172 Imazaquin 2.5 0.9988 2.5–200 2.5 84.8 12.9 50 70.7 4.5 6.5
173 Imazethapyr 1 0.9993 1–200 1 100.6 10.5 50 73.2 3.3 8.9
174 Imazosulfuron 2.5 0.9989 2.5–200 2.5 92.1 10.1 50 82.7 3.8 7.4
175 Imicyafos 10 0.9918 10–200 10 102.7 9.9 50 95.1 7.0 –4.2
176 Imidacloprid 1 0.9994 1–200 1 94.4 19.7 50 94.3 9.6 5.9
177 Inabenfide 1 0.9991 1–200 1 105.8 6.2 50 86.9 2.1 80.9
178 Indanofan 5 0.9996 5–200 5 95.9 13.7 50 92.9 4.1 4.6
179 Ipconazole 1 0.9992 1–200 1 104.6 19.8 50 85.9 3.4 –11.5
180 Iprobenfos 1 0.9993 1–200 1 76.8 17.5 50 95.0 4.4 –0.7
181 Iprovalicarb 1 0.9998 1–200 1 90.9 14.3 50 99.3 5.3 1.1
182 Isoprocarb 1 0.9999 1–200 1 97.7 12.5 50 93.8 4.7 3.7
183 Isoprothiolane 2.5 0.9989 2.5–200 2.5 94.0 14.6 50 89.1 11.7 32.2
184 Isoproturon 1 0.9998 1–200 1 97.0 7.2 50 93.0 2.2 1.8
185 Isopyrazam 2.5 0.9992 2.5–200 2.5 101.3 6.7 50 95.5 2.2 –0.7
186 Isoxaben 1 0.9987 1–200 1 99.5 10.8 50 101.9 4.3 10.5
187 Isoxathion 5 0.9980 5–200 5 74.9 4.2 50 93.3 5.0 –14.0
188 Kresoxim-methyl 10 0.9983 10–200 10 77.2 15.5 50 93.1 15.8 –13.9
189 Lenacil 1 0.9998 1–200 1 86.4 16.8 50 85.3 2.8 3.9
190 Linuron 2.5 0.9985 2.5–200 2.5 86.5 11.6 50 94.6 3.8 –0.7
191 Lufenuron 2.5 0.9993 2.5–200 2.5 105.9 15.0 50 95.8 5.2 –35.5
192 Malaoxon 10 0.9991 10–200 10 40.6 14.7 50 65.4 12.9 1.6
193 Malathion 1 0.9915 1–200 1 94.8 16.0 50 94.0 4.6 –0.1
194 Mandipropamid 1 0.9992 1–200 1 97.8 9.9 50 106.7 4.1 7.7
195 Mecarbam 1 0.9919 1–200 1 94.9 6.1 50 100.9 4.9 –4.3
196 Mefenacet 1 0.9965 1–200 1 76.4 12.6 50 96.8 4.6 –0.9
197 Mepanipyrim 1 0.9997 1–200 1 77.8 16.2 50 81.9 7.3 0.3
198 Mephosfolan 1 0.9992 1–200 1 96.1 9.8 50 96.1 3.6 6.5
199 Mepronil 1 0.9914 1–200 1 85.7 9.6 50 99.6 2.1 3.2
200 Metaflumizone 5 0.9991 5–200 5 90.2 11.6 50 93.6 3.4 –1.7
201 Metalaxyl 1 0.9998 1–200 1 97.2 9.0 50 97.0 5.4 0.2
202 Metamifop 1 0.9995 1–200 1 115.5 19.0 50 98.3 5.0 –3.4
203 Metamitron 5 0.9994 5–200 5 84.2 13.2 50 95.5 4.7 –14.1
204 Metazosulfuron 10 0.9985 10–200 10 88.2 5.3 50 91.8 5.4 0.1
205 Metconazole 1 0.9993 1–200 1 103.7 8.8 50 86.5 5.5 –9.2
206 Methabenzthiazuron 1 0.9996 1–200 1 87.0 11.9 50 89.4 4.3 1.9
207 Methamidophos 1 0.9977 1–200 1 58.6 17.1 50 62.8 6.2 13.8
208 Methiocarb 5 0.9939 5–200 5 81.9 13.0 50 92.8 4.6 24.6
209 Methiocarb sulfone 2.5 0.9985 2.5–200 2.5 92.4 13.3 50 97.1 7.5 15.8
210 Methiocarb sulfoxide 1 0.9973 1–200 1 79.9 7.1 50 90.9 6.2 5.5
211 Methomyl 1 0.9971 1–25 1 102.1 15.8 10 91.1 6.3 11.8
212 Methoprotryne 2.5 0.9964 2.5–200 2.5 73.1 7.3 50 81.2 3.0 –3.0
213 Methoxyfenozide 1 0.9981 1–200 1 85.6 19.1 50 96.2 8.1 –1.1
214 Metobromuron 1 0.9999 1–200 1 98.3 4.8 50 91.9 3.4 3.3
215 Metolcarb 5 0.9996 5–200 5 77.4 17.7 50 93.0 7.5 7.9
216 Metominostrboin (Z) 1 0.9989 1–200 1 94.1 8.6 50 100.7 2.4 –0.6
217 Metominostrobin (E) 1 0.9985 1–200 1 92.9 9.8 50 99.4 3.8 1.8
218 Metrafenon 1 0.9999 1–200 1 89.1 17.9 50 90.3 4.5 2.5
219 Mevinphos 5 0.9979 5–200 5 33.9 19.3 50 56.7 12.4 1.8
220 Monocrotophos 5 0.9989 5–200 5 49.7 13.5 50 72.5 9.3 –4.9
221 Monolinuron 1 0.9991 1–200 1 112.6 3.4 50 93.0 3.0 2.3
222 Myclobutanil 2.5 0.9979 2.5–200 2.5 109.7 16.3 50 96.8 4.7 –5.4
223 Napropamide 1 0.9991 1–200 1 72.8 7.8 50 98.9 5.5 –7.6
224 Neburon 2.5 0.9960 2.5–200 2.5 89.3 16.5 50 93.7 5.3 –2.0
225 Nicosulfuron 2.5 0.9996 2.5–200 2.5 89.9 7.3 50 77.5 5.4 25.4
226 Nitenpyram 10 0.9996 10–200 10 76.6 10.9 50 86.6 2.8 –16.1
227 Norflurazon 1 0.9980 1–200 1 97.9 6.8 50 103.4 2.6 –1.6
228 Noruron (Norea) 2.5 0.9990 2.5–200 2.5 81.2 10.3 50 84.6 5.2 2.7
229 Novaluron 5 0.9980 5–200 5 95.7 13.6 50 100.8 5.0 0.5
230 Nuarimol 2.5 0.9997 2.5–200 2.5 71.8 16.8 50 86.8 4.6 8.5
231 Ofurace 1 0.9997 1–200 1 88.9 5.1 50 92.9 4.6 11.0
232 Omethoate 1 0.9997 1–200 1 77.2 5.9 50 89.6 3.7 –10.4
233 Oxadiazon 2.5 0.9984 2.5–200 2.5 116.7 14.0 50 87.7 5.7 –0.4
234 Oxadixyl 1 0.9993 1–200 1 100.9 14.4 50 99.0 5.1 6.5
235 Oxamyl 1 0.9984 1–200 1 89.3 12.1 50 96.2 2.6 4.1
236 Oxaziclomefone 1 0.9998 1–200 1 85.4 10.6 50 89.3 3.6 –7.0
237 Paclobutrazole 2.5 0.9983 2.5–200 2.5 110.4 17.5 50 97.8 2.9 –11.1
238 Penconazole 2.5 0.9996 2.5–200 2.5 73.7 13.2 50 89.2 3.3 –7.4
239 Pencycuron 1 0.9975 1–200 1 78.6 15.9 50 93.2 2.7 –0.3
240 Penoxsulam 2.5 0.9982 2.5–200 2.5 84.9 4.1 50 98.3 4.0 0.2
241 Pentoxaone 10 0.9933 10–200 10 76.2 13.4 50 78.4 4.8 1.1
242 Phenthoate 2.5 0.9976 2.5–200 2.5 99.9 11.6 50 98.3 6.2 –0.2
243 Phosalone 2.5 0.9973 2.5–200 2.5 86.0 10.2 50 89.6 6.0 2.9
244 Phosfolan 1 0.9995 1–200 1 84.9 17.3 50 92.6 6.0 6.1
245 Phosphamidon 1 0.9997 1–200 1 104.4 6.9 50 90.5 7.3 –1.9
246 Phoxim 1 0.9978 1–200 1 83.7 19.4 50 94.5 3.4 –10.3
247 Picolinafen 1 0.9997 1–200 1 80.0 19.5 50 84.2 1.6 –33.5
248 Picoxystrobin 2.5 0.9995 2.5–200 2.5 102.0 7.6 50 102.6 4.9 –12.6
249 Piperonyl butoxide 1 0.9995 1–200 1 90.3 14.4 50 93.7 6.4 –11.9
250 Piperophos 1 0.9992 1–200 1 92.2 8.9 50 96.2 6.3 –1.4
251 Pirimicarb 1 0.9968 1–200 1 71.2 7.0 50 77.2 3.2 3.3
252 Pirimicarb-desmethyl 5 0.9996 5–200 5 68.1 11.4 50 80.1 10.6 0.4
253 Pirimiphos-ethyl 1 0.9971 1–200 1 86.1 12.1 50 89.4 5.0 –17.9
254 Pirimiphos-methyl 1 0.9989 1–200 1 89.7 8.5 50 87.2 2.9 –4.0
255 Probenazole 10 0.9962 10–200 10 101.6 10.4 50 103.0 4.8 3.9
256 Prochloraz 10 0.9996 10–200 10 74.8 5.5 50 78.5 2.1 –2.0
257 Profenofos 2.5 0.9994 2.5–200 2.5 75.6 5.1 50 88.3 2.5 –2.0
258 Promecarb 1 0.9993 1–200 1 90.9 12.2 50 92.7 5.1 1.7
259 Prometryn 1 0.9969 1–200 1 68.7 4.5 50 74.2 7.7 0.5
260 Pronamide (Propyzamide) 2.5 0.9977 2.5–200 2.5 98.1 13.0 50 95.1 3.4 4.5
261 Propachlor 1 0.9996 1–200 1 81.9 8.4 50 84.4 2.6 –0.3
262 Propamocarb 1 0.9996 1–200 1 83.2 6.0 50 91.5 2.6 –3.8
263 Propanil 5 0.9987 5–200 5 91.3 8.5 50 87.3 3.4 –8.4
264 Propaquizafop 5 0.9996 5–200 5 85.2 7.8 50 93.1 1.2 –19.8
265 Propargite 1 1.0000 1–200 1 88.6 3.9 50 90.0 1.9 –9.9
266 Propazine 1 0.9993 1–200 1 86.1 16.4 50 79.9 9.0 –14.8
267 Propiconazole 2.5 0.9995 2.5–200 2.5 92.1 19.6 50 89.6 6.1 –5.3
268 Propoxur 1 0.9943 1–200 1 91.1 11.7 50 99.9 7.7 –4.5
269 Proqunazid 1 0.9998 1–200 1 55.3 3.0 50 57.1 1.1 –5.8
270 Prosulfocarb 1 0.9990 1–200 1 89.8 13.0 50 81.1 2.6 13.2
271 Prothioconazole-desthio 5 0.9992 5–200 5 86.7 14.8 50 84.4 5.4 −18.4
272 Pydiflumetofen 2.5 0.9984 2.5–200 2.5 93.4 9.7 50 93.8 4.4 −3.6
273 Pyracarbolid 1 0.9935 1–200 1 86.6 5.4 50 100.6 4.8 0.8
274 Pyraclofos 1 0.9993 1–200 1 85.8 8.7 50 97.8 4.5 9.3
275 Pyraclonil 1 0.9972 1–200 1 98.3 6.8 50 96.2 6.0 7.7
276 Pyraclostrobin 2.5 0.9988 2.5–200 2.5 103.8 14.7 50 97.4 3.6 −15.3
277 Pyraflufen-ethyl 1 0.9974 1–200 1 78.4 16.7 50 93.6 6.7 7.3
278 Pyraziflumid 1 0.9990 1–200 1 115.8 13.9 50 97.3 5.4 9.6
279 Pyrazolate 5 0.9991 5–200 5 95.9 8.5 50 95.2 3.2 2.2
280 Pyrazophos 1 0.9972 1–200 1 87.5 7.7 50 96.4 3.1 31.6
281 Pyribenzoxim 2.5 0.9900 2.5–200 2.5 103.9 19.0 50 97.4 14.3 −16.0
282 Pyributicarb 1 0.9993 1–200 1 87.5 4.3 50 84.1 4.4 −14.1
283 Pyridaben 1 0.9996 1–200 1 74.9 4.0 50 77.9 1.9 1.0
284 Pyridalyl 10 0.9997 10–200 10 55.3 15.6 50 58.3 3.0 −17.2
285 Pyridaphenthion 1 0.9993 1–200 1 91.5 8.2 50 101.9 11.6 −0.6
286 Pyridate 2.5 0.9964 2.5–200 2.5 105.4 3.7 50 73.9 1.2 4.5
287 Pyrifluquinazon 2.5 0.9968 2.5–200 2.5 75.3 8.0 50 87.6 3.1 −4.6
288 Pyriftalid 1 0.9976 1–200 1 86.2 12.0 50 97.2 6.4 −4.0
289 Pyrimethanil 2.5 0.9993 2.5–200 2.5 64.6 6.7 50 58.9 9.5 −1.8
290 Pyrimidifen 1 0.9993 1–200 1 54.6 16.4 50 67.0 3.1 −46.0
291 Pyriminobac (E) 1 0.9975 1–200 1 100.2 8.9 50 112.6 5.2 −7.9
292 Pyriminobac (Z) 1 0.9939 1–200 1 90.4 5.1 50 106.9 6.7 −4.9
293 Pyrimisulfan 1 0.9998 1–200 1 95.1 11.8 50 95.2 6.0 7.4
294 Pyriproxyfen 1 0.9994 1–200 1 79.2 7.0 50 82.8 5.4 −6.2
295 Pyroquilon 1 0.9994 1–200 1 79.2 19.7 50 91.3 5.4 2.6
296 Quinalphos 5 0.9964 5–200 5 87.5 11.8 50 89.8 2.0 2.0
297 Quinoclamine 10 0.9979 10–200 10 74.1 13.1 50 84.5 5.7 −4.1
298 Quizalofop-ethyl 1 0.9985 1–200 1 70.6 15.1 50 88.3 3.0 −3.4
299 Saflufenacil 2.5 0.9980 2.5–200 2.5 100.9 12.7 50 99.9 6.2 13.2
300 Sethoxydim A 2.5 0.9998 2.5–200 2.5 77.8 3.2 50 80.5 2.2 −3.3
301 Simazine 1 0.9993 1–200 1 87.4 17.9 50 90.0 2.9 1.6
302 Simeconazole 2.5 0.9988 2.5–200 2.5 108.9 10.3 50 95.8 4.5 −2.8
303 Simetryn 1 0.9998 1–200 1 75.6 9.7 50 74.2 4.5 −5.4
304 Spinetoram (J) 1 0.9986 1–200 1 87.9 18.7 50 101.7 17.8 −10.6
305 Spinetoram (L) 1 0.9993 1–200 1 90.4 11.5 50 102.0 4.0 −7.3
306 Spinosyn A 1 0.9978 1–200 1 96.1 14.4 50 87.4 4.1 −6.6
307 Spinosyn D 5 0.9995 5–200 5 108.7 10.3 50 98.8 3.8 −17.0
308 Spirodiclofen 2.5 0.9998 2.5–200 2.5 91.3 4.0 50 85.1 1.6 6.9
309 Spirotetramat 2.5 0.9985 2.5–200 2.5 80.8 13.1 50 101.0 7.6 4.7
310 Spirotetramat-enol 1 0.9988 1–200 1 92.2 10.0 50 90.2 4.1 1.5
311 Spirotetramat-enol-glucoside 10 0.9933 10–200 10 112.2 6.3 50 69.2 4.7 −11.6
312 Spirotetramat-ketohydroxy 10 0.9997 10–200 10 92.1 7.8 50 90.5 2.9 6.0
313 Spirotetramat-monohydroxy 2.5 0.9978 2.5–200 2.5 78.5 17.5 50 96.6 6.3 −4.3
314 Spiroxamine 1 0.9986 1–200 1 82.5 7.2 50 91.5 4.9 0.6
315 Sulfentrazone 2.5 0.9951 2.5–200 2.5 105.8 9.7 50 106.7 4.8 4.7
316 Sulfotep 1 0.9982 1–200 1 87.4 17.3 50 95.6 3.2 3.0
317 Sulfoxaflor 1 0.9976 1–200 1 91.8 3.5 50 99.5 2.5 37.1
318 Sulprofos 2.5 0.9999 2.5–200 2.5 86.6 12.4 50 83.3 1.1 3.7
319 TCMTB 10 0.9993 10–200 10 15.8 18.0 50 16.1 4.9 −6.7
320 Tebuconzole 2.5 0.9989 2.5–200 2.5 90.9 10.4 50 88.6 6.1 13.9
321 Tebufenozide 2.5 0.9912 2.5–200 2.5 97.2 10.6 50 103.7 15.1 −15.8
322 Tebufenpyrad 2.5 0.9997 2.5–200 2.5 88.3 11.1 50 82.4 2.9 −26.6
323 Tebuthiuron 1 0.9990 1–200 1 90.9 14.9 50 89.3 7.3 −2.9
324 Teflubenzuron 1 0.9998 1–200 1 91.3 13.7 50 85.0 4.3 77.3
325 Tepraloxydim 2.5 0.9967 2.5–200 2.5 98.6 19.1 50 98.0 6.7 −1.7
326 Terbuthylazine 2.5 0.9996 2.5–200 2.5 77.5 3.5 50 79.0 5.1 −2.4
327 Terbutryn 10 0.9938 10–200 10 65.9 3.2 50 72.8 2.4 1.3
328 Tetrachlorvinphos 10 0.9999 10–200 10 48.2 7.9 50 70.1 8.6 2.6
329 Tetraconazole 1 0.9996 1–200 1 112.7 17.3 50 97.1 2.6 −7.3
330 Thenylchlor 2.5 0.9990 2.5–200 2.5 89.9 9.2 50 97.4 3.8 −3.8
331 Thiabendazole 1 0.9993 1–200 1 69.0 10.4 50 67.0 3.9 8.2
332 Thiacloprid 1 0.9976 1–200 1 89.7 13.5 50 102.6 3.6 9.7
333 Thiamethoxam 2.5 0.9991 2.5–200 2.5 71.2 17.7 50 97.0 2.1 −5.0
334 Thiazopyr 2.5 0.9982 2.5–200 2.5 89.3 11.4 50 98.9 5.7 0.8
335 Thidiazuron 1 0.9995 1–200 1 76.9 5.2 50 79.8 5.3 14.9
336 Thifensulfuron-methyl 1 0.9998 1–200 1 77.9 13.6 50 82.8 1.5 12.0
337 Thifluzamide 10 0.9948 10–200 10 99.2 16.7 50 105.8 8.1 9.8
338 Thiobencarb 1 0.9997 1–200 1 96.3 15.4 50 80.0 4.6 5.6
339 Thionazin 1 0.9993 1–200 1 108.1 11.1 50 97.7 3.2 1.8
340 Tiadinil 1 0.9994 1–200 1 91.2 5.4 50 84.1 2.8 16.8
341 Tolfenpyrad 2.5 0.9996 2.5–200 2.5 83.7 14.0 50 84.5 5.5 −13.0
342 Triadimefon 5 0.9983 5–200 5 88.6 14.7 50 97.3 4.0 3.0
343 Triazophos 1 0.9947 1–200 1 99.9 11.7 50 116.8 3.6 −7.4
344 Tricyclazole 1 0.9973 1–200 1 79.4 9.1 50 84.5 6.8 −0.3
345 Trifloxystrobin 1 0.9989 1–200 1 118.6 11.1 50 102.7 3.3 −12.2
346 Triflumizole 1 0.9994 1–200 1 89.2 12.4 50 81.5 6.4 −13.5
347 Triflumuron 2.5 0.9998 2.5–200 2.5 96.1 9.8 50 94.2 2.9 −8.6
348 Trimethacarb 1 0.9998 1–200 1 98.3 7.4 50 91.2 2.1 5.1
349 Triticonazole 2.5 0.9995 2.5–200 2.5 75.7 17.3 50 92.6 2.2 −6.3
350 Uniconazole 2.5 0.9990 2.5–200 2.5 82.8 9.7 50 96.7 8.1 −19.3
351 Vamidothion 1 0.9987 1–200 1 82.2 8.9 50 95.0 7.5 −1.1
352 XMC 1 0.9992 1–200 1 90.4 14.1 50 93.2 2.6 13.1
353 Zoxamide 1 0.9989 1–200 1 92.6 19.1 50 100.7 7.1 −2.8

1 Concentration of treatment. 2 Matrix effect.