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. 2020 Dec 15;11:595692. doi: 10.3389/fphar.2020.595692

TABLE 5.

Stability of the UHPLC-MS method determined using QC samples.

No. t R/min RSD (%) RSD of relative peak areas/% m/z Ion RSD (%)
1 1.28 1.1405 19.43 215.0398 [M−H] 2.94 × 10–5
2 1.60 1.1037 25.06 132.0946 [M+H]+ 3.09 × 10–5
3 6.63 0.3424 12.84 723.5102 [M−H] 1.62 × 10–5
4 11.21 0.5977 11.86 274.2665 [M+H]+ 1.88 × 10–5
5 16.74 0.3019 3.11 520.3325 [M+H]+ 2.55 × 10–5
6 16.87 0.3404 9.27 588.3383 [M−H] 1.78 × 10–5
7 17.17 0.3313 7.57 496.3324 [M+H]+ 2.36 × 10–5
8 17.79 0.2863 8.00 540.3384 [M−H] 2.16 × 10–5
9 18.75 0.2759 6.87 522.3482 [M+H]+ 3.30 × 10–5
10 21.35 0.3165 5.54 524.3639 [M+H]+ 2.23 × 10–5