Skip to main content
. 2021 Jan 3;1230:129868. doi: 10.1016/j.molstruc.2020.129868

Table 5.

Ultrasound assisted synthesis of compound 3c-j.a

Image, table 5
1; R’, R = Time Product (3) %Yieldb
1a; H, Ph 1.5 3c 67
1b; H, C6H4Me-p 1.5 3d 71
1c; H, t-Bu 2 3e 59
1d; H, CMe2OH 1.5 3f 63
1e; H, n-Bu 1.5 3g 73
1f; H, H 2 3h 60
1g; Me. Ph 4 3i 65
1h; Me, C6H4Me-p 1.5 3j 62
a

All the reactions were carried out by using 1 (2.5 mmol), 2d (2.8 mmol), Cu(OAc)2 (0.025 mmol) and Et3N (3.77 mmol) in DMF (3 mL) under ultrasound.

b

Isolated yield.