Table 2. Hydrogen-bond geometry (Å, °) for (1).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| O1—H1⋯O10 | 0.85 (1) | 1.78 (1) | 2.627 (3) | 173 (4) |
| O1—H2⋯O7i | 0.85 (1) | 1.85 (1) | 2.689 (3) | 171 (4) |
| O2—H3⋯O8ii | 0.85 (1) | 1.84 (1) | 2.684 (3) | 176 (4) |
| O2—H4⋯OW1 | 0.85 (1) | 1.76 (1) | 2.600 (3) | 171 (4) |
| O3—H5⋯O7iii | 0.85 (1) | 1.83 (1) | 2.675 (3) | 178 (4) |
| O3—H6⋯O9i | 0.85 (1) | 1.83 (1) | 2.670 (3) | 169 (4) |
| O4—H7⋯O8iv | 0.85 (1) | 1.91 (1) | 2.745 (3) | 168 (4) |
| O4—H8⋯O11v | 0.85 (1) | 2.12 (2) | 2.884 (4) | 150 (4) |
| O4—H8⋯O13v | 0.85 (1) | 2.13 (3) | 2.870 (4) | 147 (4) |
| O5—H9⋯O9vi | 0.85 (1) | 1.80 (1) | 2.650 (3) | 179 (4) |
| O5—H10⋯O10iv | 0.85 (1) | 1.79 (1) | 2.640 (3) | 175 (4) |
| O6—H11⋯OW2 | 0.85 (1) | 1.79 (2) | 2.596 (4) | 160 (4) |
| O6—H12⋯O11vii | 0.85 (1) | 2.35 (3) | 3.044 (4) | 139 (3) |
| O6—H12⋯O12vii | 0.85 (1) | 2.06 (2) | 2.876 (4) | 162 (4) |
| OW1—H13⋯O13 | 0.86 (1) | 2.05 (2) | 2.850 (5) | 155 (3) |
| OW1—H14⋯O12vii | 0.86 (1) | 2.52 (4) | 3.109 (5) | 127 (4) |
| OW1—H14⋯OW2viii | 0.86 (1) | 2.55 (4) | 3.073 (6) | 120 (3) |
| OW2—H16⋯O12viii | 0.86 (1) | 2.20 (3) | 2.908 (5) | 139 (3) |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
; (viii)
.